Joint detection kit, detection method and immunoassay system
A combined detection and kit technology, applied in the field of immune detection, can solve the problems of consumption, increased cost, hospital and patient burden, and achieve the effect of improving detection efficiency
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Embodiment 1
[0076] Preparation of capture antibody composition
[0077] 1) Select two types of microspheres with a particle size of 5.5 μm and 8 μm, the 5.5 μm microspheres are coated with mouse anti-human PCT antibody, and the 8 μm microspheres are coated with mouse anti-human IL-6 antibody;
[0078] 2) 1 mg of magnetic fluorescent-encoded microspheres were magnetically separated using a magnetic separation plate, and the supernatant was absorbed;
[0079] 3) Add 1 mL of 50 mM, pH 6.0 2-morpholineethanesulfonic acid (MES) buffer solution, vortex the microspheres for 20 s, perform magnetic separation with a magnetic separation plate, and absorb the supernatant. This step is repeated three times;
[0080] 4) Add 2 mL of the above-mentioned MES buffer solution, vortex the microspheres for 20 seconds, and add 10 μL of 50 mg / mL N-hydroxysuccinimide (NHS) and 1-(3- Dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride (EDC) solution, incubate with shaking at room temperature for 20 min, per...
Embodiment 2
[0096] Preparation of capture antibody composition
[0097] 1) Two kinds of encoded magnetic fluorescent microspheres with different encodings are selected and coated with mouse anti-human PCT antibody and mouse anti-human IL-6 antibody respectively;
[0098] 2) 0.5 mg of magnetic fluorescence-encoded microspheres were magnetically separated using a magnetic separation plate, and the supernatant was absorbed;
[0099] 3) Add 1mL of 20mM, pH 7.0 N-(2-hydroxyethyl)piperazine-N'-2-ethanesulfonic acid (HEPES) buffer solution, vortex the microspheres for 20s, and use a magnetic separation plate Magnetically separate and aspirate the supernatant. This step is repeated three times;
[0100]4) Add 1 mL of the above-mentioned HEPES buffer, vortex the microspheres for 20 seconds, add 5 μL of 50 mg / mL N-hydroxysuccinimide (NHS) and 1-(3 -Dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride (EDC) solution, then add 20 μg of the corresponding antibody to the solution, incubate with sh...
Embodiment 3
[0115] Preparation of capture antibody composition
[0116] 1) Two kinds of encoded magnetic fluorescent microspheres with different encodings are selected and coated with goat anti-human PCT antibody and rabbit anti-human IL-6 antibody respectively;
[0117] 2) 1.0 mg of magnetic fluorescence-encoded microspheres were magnetically separated using a magnetic separation plate, and the supernatant was absorbed;
[0118] 3) Add 1 mL of 20 mM boric acid (BS) buffer solution with pH 8.0, vortex the microspheres for 20 s, perform magnetic separation with a magnetic separation plate, and absorb the supernatant. This step is repeated three times;
[0119] 4) Add 2 mL of the above-mentioned boric acid buffer solution, vortex the microspheres for 20 seconds, add 5 μL of 100 mg / mL N-hydroxysuccinimide (NHS) and 1-(3 -Dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride (EDC) solution, then add 20 μg of the corresponding antibody to the solution, incubate with shaking at room temperat...
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