Continuous collection device, preparation device and preparation method of carbon nanotube film
A technology of carbon nanotube film and collection device, which is applied in lighting and heating equipment, thin material processing, transportation and packaging, etc., can solve the problems of poor continuity and low efficiency, achieve continuous production and reduce manual operation process Effect
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[0072] The present invention also discloses a continuous preparation method of carbon nanotube film, the preparation method adopts the above-mentioned continuous preparation device of carbon nanotube film, refer to Figure 1 to Figure 6 Shown, this preparation method comprises the following steps:
[0073] The carbon nanotube macroscopic body is produced by floating catalytic chemical vapor deposition, and the carbon nanotube macroscopic body is blown out from the outlet end of the furnace tube through the carrier gas.
[0074] The carbon nanotube macroscopic body is automatically and continuously wound on its surface by a rotating collecting drum. In this step, the carbon nanotube macroscopic bodies may be uniformly arranged in multiple rows along the axial direction of the collection drum, and at the same time may be arranged in multiple layers along the radial direction of the collection drum.
[0075] After the collection of the carbon nanotube macroscopic body is complet...
Embodiment 1
[0083] 1. Clean the inside of the box, close the flip door, close the sealing system of the furnace mouth, and close the solenoid valve to ensure the inside of the box is sealed.
[0084] 2. Turn on the vacuum pump, and use protective gases such as argon and nitrogen to discharge the air inside the box from the exhaust system through the replacement method, so as to reduce the oxygen content inside the box to a safe range.
[0085] 3. Turn off the vacuum pump, open the furnace mouth sealing system, open the solenoid valve, and at the same time pass protective inert gases such as argon or nitrogen into the box, and then pass carbon source gas or liquid into the interior from the entrance section of the high-temperature furnace tube. Catalyst, hydrogen, argon and other carrier gases are used to produce carbon nanotubes by the floating catalytic chemical vapor deposition method. The carrier gas will blow out the cylindrical macroscopic body of carbon nanotubes formed and assembled i...
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