Alkali-process zinc powder combined smelting method
A smelting method and zinc powder technology are applied in the field of combined alkaline zinc powder smelting, which can solve the problems of expensive equipment, harsh operating environment and high cost, and achieve the effect of solving expensive equipment.
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[0059] A smelter adopts a hydrometallurgical method and a three-stage antimony purification method to achieve deep purification.
[0060] The analysis of the new electrolytic solution is as follows, the unit is mg / L, and the unit of Zn is g / L,
[0061] Zn Fe Sb Cd co Ge pH Liquid 1 139.62 6.28 0.003 0.03 0.10 0.006 4.95
[0062] Use 3L of electrolytic new solution, add appropriate amount of caustic soda to obtain a zinc precipitation solution with pH = 7, obtain zinc precipitation residue after filtration, and put the zinc precipitation filter residue into the zinc precipitation filter residue with an initial concentration of 6mol / L according to the ratio of liquid to solid ratio of 8:1 In NaOH solution, stir at 50°C for 1 hour to obtain an alkaline immersion solution, which is directly used in alkaline electrolysis. After electrolysis for 2 hours, the obtained alkaline zinc powder is collected, filtered, and washed. 10%, 15%, and 20% w...
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