Method for determining rock sealing stress
A technique for determining methods, rocks, applied in the field of geological surveys to achieve high accuracy
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[0070] (1) Rock sample processing
[0071] Quartz vein rocks were cut along the rock plane and vertical plane, and the sample size was 20mm×20mm×10mm. The way to establish its coordinate system is as follows: figure 2 shown.
[0072] (2) Determination of rock quartz content by cathodoluminescence
[0073] The quartz content was calculated by cathodoluminescence microscopy and Image J software.
[0074] (3) Obtain sample X-ray diffraction spectrum
[0075] Equipment parameters: Bruker D8 Advance X-ray diffractometer, equipped with Yula ring, using Cu target, wavelength Focus spot, working voltage and current: 40kV, 40mA; optical path: focusing optical path-Ni filter-collimator tube 2.0mm.
[0076] Perform a full spectrum scan of the assay point. Angle range: 10°-158°, scanning step: 0.1°, dwell time per step: 0.15s.
[0077] (4) Select the measurement crystal plane
[0078] Perform a phase search, match the #99-0088PDF card, and select the (132) crystal plane for meas...
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