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Nanofiber filtering membrane as well as preparation method and application thereof

A nanofiber and filter membrane technology, applied in the field of aerosol protection, can solve the problems of inability to achieve high-efficiency aerosol capture and poor aerosol protection effect, and achieve excellent antibacterial performance, self-cleaning performance, and low filter resistance.

Pending Publication Date: 2021-10-01
TAIZHOU RES INST OF SOUTHERN UNIV OF SCI & TECH +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

All the nanofiber-microfiber composite anti-fog masks have poor protective effect on aerosols and cannot achieve efficient capture of aerosols

Method used

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  • Nanofiber filtering membrane as well as preparation method and application thereof
  • Nanofiber filtering membrane as well as preparation method and application thereof
  • Nanofiber filtering membrane as well as preparation method and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0058] The present embodiment provides a kind of nanofiber filter membrane, and its preparation method is as follows:

[0059] Preparation of nanofiber filter membrane: Weigh SiO 2 Slowly add dimethylformamide (DMF), place in an ultrasonic cleaner for 1h to make SiO 2 After uniform dispersion, add PVDF powder with a molecular weight of 200,000, place it on a thermal magnetic stirrer, heat to 50°C and stir for more than 2 hours until the PVDF is completely dissolved, then weigh ZnAc·2H 2 O is added, heated and magnetically stirred to obtain PVDF+SiO 2 (5%)+ZnAc·2H 2 O (5%) solution (percent represents SiO 2 The mass proportion is 5%, ZnAc·2H 2 The mass proportion of O is 10%). Using electrospinning method, take PVDF+SiO 2 +ZnAc·2H 2 O The spinning liquid is poured into the syringe, and the PP non-woven fabric is used as the receiving substrate. In an environment with a temperature of 25°C and a humidity of 50%, apply a high voltage of 18kV, adjust the spinning distance t...

Embodiment 2

[0064] The only difference from Example 1 is that SiO in the spinning solution 2 and ZnAc·2H 2 The mass proportion of O is different, specifically PVDF+SiO 2 (5%)+ZnAc·2H 2 O (10%), the SEM test result of nanofiber filter membrane is as figure 2 shown.

[0065] The above-mentioned nanofiber filter membrane was tested, and the experimental results showed that the aerosol filter efficiency was 93.2%, and the air resistance was 115Pa.

Embodiment 3

[0067] The only difference from Example 1 is that SiO in the spinning solution 2 and ZnAc·2H 2 The mass proportion of O is different, specifically PVDF+SiO 2 (5%)+ZnAc·2H 2 O (20%), the SEM test result of nanofiber filter membrane is as image 3 shown.

[0068] The above-mentioned nanofiber filter membrane is tested, and the experimental results show that the aerosol filter efficiency is 95%, and the air resistance is 145Pa.

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Abstract

The invention relates to a nanofiber filtering membrane as well as a preparation method and application thereof. The nanofiber filtering membrane comprises polymer fibers, and electret nanoparticles and ZnAc.2H2O which are attached to the surfaces of the polymer fibers. The ZnAc.2H2O and the electret nanoparticles have a synergistic effect, so that the electret effect of the electret nanoparticles can be effectively promoted, the nanofiber membrane can more efficiently capture aerosol with smaller diameter, the nanofiber membrane has lower filter resistance, namely, has high efficiency and low resistance, and meanwhile, the antibacterial performance of the nanofiber membrane can be effectively improved. The nanofiber filtering membrane can be used in protective articles such as masks and protective clothing.

Description

technical field [0001] The invention relates to the technical field of aerosol protection, in particular to a nanofiber filter membrane and its preparation method and application, in particular to a nanofiber filter membrane for efficiently capturing aerosols and its preparation method and application. Background technique [0002] Aerosols are droplets with a diameter of less than 5 microns. Smaller, lighter aerosols can stay and accumulate in the air, and if the aerosols contain viruses, they can travel long distances under the action of air currents, leading to disease. Therefore, research on the effective interception of aerosols is particularly important. [0003] At present, nanofiber filter membranes in the prior art have higher filtration efficiency than conventional nonwoven filter membranes due to their small diameter, high porosity, and large specific surface area, and are widely used in air filtration, sewage filtering etc. However, with the development of the...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01D71/68B01D71/64B01D71/58B01D71/42B01D71/38B01D71/30B01D69/08B01D69/02B01D67/00B01D46/54
CPCB01D71/30B01D71/42B01D71/68B01D71/64B01D71/38B01D71/58B01D69/08B01D69/02B01D67/0079B01D46/543B01D2325/48
Inventor 陈柔羲王湘麟陈明伊陈健朱自辉曾元张化
Owner TAIZHOU RES INST OF SOUTHERN UNIV OF SCI & TECH