Fractal crystal of cyano-substituted spirocyclic aromatic hydrocarbon molecules, and preparation method and application of fractal crysta
A technology of spiro aromatic hydrocarbons and cyano substitution, applied in the field of cyano substituted spiro aromatic hydrocarbon molecular fractal crystals and its preparation, to achieve good shape stability and luminescence stability, uniform size, and good crystallinity
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Embodiment 1- Embodiment 5
[0039] Embodiment 1-Example 5: Preparation method of TCN-SFX fractal crystal
[0040] Weigh a certain mass of TCN-SFX sample into a 10mL sample bottle, add 1mL tetrahydrofuran to fully dissolve, and configure a TCN-SFX tetrahydrofuran solution with a concentration range of 4-8mM, quickly inject the TCN-SFX tetrahydrofuran solution into a vigorously stirred 5mL SDS In the sample bottle of the aqueous solution, cover the lid and stir for 5 minutes, take out the magnet, and stand still at 40-80° C. for 72 hours to obtain a suspension of fractal crystals. The fractal crystals can be obtained after the solvent evaporates.
[0041]Embodiment 1-Example 5, the difference between different embodiments is only the sample concentration and the preparation environment temperature, the remaining parameters and steps are the same, the specific sample concentration and preparation environment setting conditions of each embodiment are detailed in the following table:
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