Electrothermal coating slurry, preparation method and application
A coating slurry and electric heating technology, applied in the direction of conductive coatings, coatings, etc., can solve the problems that cannot be used for industrial heating, easy to produce toxic and harmful gases, and current path breaks, etc., to achieve stable electrical performance, long working life, coating layer hydrophobic effect
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[0050] The second aspect of the present application provides a method for preparing an electrothermal coating slurry, the method comprising:
[0051] Step 1, adding an acidic substance to the dispersion of the conductive substance, adjusting the pH to 4-5 to obtain a mixture I;
[0052] Step 2. Mix the mixture I with the silane solution and react to obtain the electrothermal coating slurry, specifically:
[0053] Step 2.1. After mixing the mixture I and the silane solution evenly, adjust the pH to 4-5 with an acidic substance to obtain the mixture II; the solvent of the silane solution is at least one selected from ethanol and water.
[0054] Step 2.2, mix the mixture II and the graphene dispersion evenly, and react to obtain the electrothermal coating slurry.
[0055] Wherein the reaction condition is:
[0056] The reaction temperature is 20~30℃, and the reaction time is 3~4h.
[0057] After mixing the mixture I and the silane solution uniformly in the above step 2.1, use ...
Embodiment 1
[0067] The electrothermal coating slurry of this embodiment includes the components shown in Table 1.
[0068] Table 1 The first component of electrothermal coating slurry
[0069] raw material name Specification Amount added indium tin oxide 80nm 3 parts by weight n-octyltrimethoxysilane 99% 2.7 parts by weight glacial acetic acid Analytical pure 0.1 parts by weight ethanol Analytical pure 10.8 parts by weight ionized water self made 60 parts by weight
[0070] The preparation method of the above-mentioned electrothermal coating slurry is as follows:
[0071] Step 1. Weigh indium tin oxide and place it in a plastic beaker, add glacial acetic acid dropwise to adjust the pH value to 4.5, stop adding glacial acetic acid, and obtain mixture I;
[0072] Step 2. Mix ethanol and n-octyltrimethoxysilane, then add deionized water, stir evenly, and add the mixture I in step 1 into it. Adjust the pH of the mixed solution to ...
Embodiment 2
[0075] The electrothermal coating slurry of this embodiment includes the components shown in Table 2.
[0076] Table 2 The second component of electrothermal coating slurry
[0077] raw material name Specification Amount added indium tin oxide 80nm 6 parts by weight silica 30nm 5 parts by weight n-octyltrimethoxysilane 99% 5.5 parts by weight glacial acetic acid Analytical pure 0.5 parts by weight ethanol Analytical pure 22 parts by weight ionized water self made 70 parts by weight
[0078] The preparation method of the above-mentioned electrothermal coating slurry is as follows:
[0079] Step 1. Weigh indium tin oxide and silicon dioxide according to the prescription and place them in a plastic beaker, add glacial acetic acid dropwise to adjust the pH value to 4.5, stop adding glacial acetic acid, and obtain mixture I;
[0080] Step 2. Mix ethanol and n-octyltrimethoxysilane, then add deionized water, stir...
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