A kind of antibacterial and antistatic fiber coating and preparation method thereof
An antistatic fiber and coating technology, applied in fiber treatment, biochemical fiber treatment, textiles and papermaking, etc.
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Embodiment 1
[0040] An antibacterial and antistatic fiber coating and a preparation method thereof, in parts by weight, mainly include: 2 parts of modified carboxymethyl chitosan quaternary ammonium salt and 16 parts of aminated modified graphene.
[0041] A preparation method of an antibacterial and antistatic fiber coating, the preparation method of the antibacterial and antistatic fiber coating mainly comprises the following preparation steps:
[0042] (1) Add carboxymethyl chitosan into a three-necked flask with a stirring and refluxing device, add 7 times the mass of carboxymethyl chitosan in isopropanol and 1 times the mass of carboxymethyl chitosan in 40% hydroxide Aqueous sodium solution, stirred and heated in a water bath to raise the temperature of the material to 45.0 °C, and continued to stir and alkalize for 1 h to obtain a mixed solution; then slowly add 40% mass fraction of 3-chlorine to the mixed solution at 15 drops / min dropwise. -2 hydroxypropyltrimethylammonium chloride ...
Embodiment 2
[0053] An antibacterial and antistatic fiber coating and a preparation method thereof, in parts by weight, mainly include: 2 parts of carboxymethyl chitosan quaternary ammonium salt and 16 parts of aminated modified graphene.
[0054] A preparation method of an antibacterial and antistatic fiber coating, the preparation method of the antibacterial and antistatic fiber coating mainly comprises the following preparation steps:
[0055] (1) Add carboxymethyl chitosan into a three-necked flask with a stirring and refluxing device, add 7 times the mass of carboxymethyl chitosan in isopropanol and 1 times the mass of carboxymethyl chitosan in 40% hydroxide Aqueous sodium solution, stirred and heated in a water bath to raise the temperature of the material to 45.0 °C, and continued to stir and alkalize for 1 h to obtain a mixed solution; then slowly add 40% mass fraction of 3-chlorine to the mixed solution at 15 drops / min dropwise. -2 hydroxypropyltrimethylammonium chloride solution,...
Embodiment 3
[0064] An antibacterial and antistatic fiber coating and a preparation method thereof, in parts by weight, mainly include: 2 parts of modified carboxymethyl chitosan quaternary ammonium salt, and 16 parts of graphene oxide.
[0065] A preparation method of an antibacterial and antistatic fiber coating, the preparation method of the antibacterial and antistatic fiber coating mainly comprises the following preparation steps:
[0066] (1) Add carboxymethyl chitosan into a three-necked flask with a stirring and refluxing device, add 7 times the mass of carboxymethyl chitosan in isopropanol and 1 times the mass of carboxymethyl chitosan in 40% hydroxide Aqueous sodium solution, stirred and heated in a water bath to raise the temperature of the material to 45.0 °C, and continued to stir and alkalize for 1 h to obtain a mixed solution; then slowly add 40% mass fraction of 3-chlorine to the mixed solution at 15 drops / min dropwise. -2 hydroxypropyltrimethylammonium chloride solution, t...
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