4results about How to "Uniform size distribution" patented technology

The invention discloses a method for continuously preparing a chiral enriched single-walled carbon nanotube by adopting a fluidized bed, and belongs to the technical field of carbon nanotubes. The method comprises the following steps: preparing a fluidized catalyst by a sol-gel method, mixing a metal catalyst salt, an inorganic sol carrier, a pore-forming template agent and an electrolyte gel to form gel, and drying and annealing to form the fluidized catalyst with the particle size of 50-200 microns and rich mesopores; the method comprises the following steps: reducing and activating a catalyst in a pretreatment reactor, introducing into a main reactor, introducing a carbon source gas and a carrier gas, and cracking and depositing a carbon source at an active center of the catalyst to grow a single-walled carbon nanotube; after the growth is finished, increasing the carrier gas flow and conveying a product to a cooling separator for collection; and after the main reactor is empty, the next batch of catalyst can be introduced without cooling to realize continuous preparation. According to the method, the catalyst metal is uniformly dispersed, the fluidization performance is excellent, the growth of multi-wall and large-diameter carbon nanotubes can be effectively inhibited, and the efficient and continuous preparation of the chiral enriched single-wall carbon nanotubes is realized.

This invention belongs to the field of materials preparation and discloses a method for preparing plate-like zinc phosphate, comprising the following steps: (1) adding an inducing agent to a phosphoric acid solution; (2) adding the mixed solution from step (1) to a zinc oxide slurry, stirring the mixture at 60-90°C, and filtering and drying the reaction product after the reaction to obtain plate-like zinc phosphate. This invention directly controls the growth morphology of plate-like crystals through an aqueous synthesis reaction, eliminating the need for ultrafine grinding, reducing process flow and equipment investment, lowering energy consumption per unit product, and meeting the requirements of green manufacturing.

This invention discloses a nanocomposite phase change antifreeze water-reducing agent and its preparation method, comprising water and the following components in parts by weight: 5-8 parts polycarboxylate superplasticizer mother liquor, 6-10 parts ethylene glycol, 8-10 parts calcium formate, 2-4 parts sodium nitrite, 5-8 parts methanol, 2-5 parts sodium metasilicate, 1-2 parts sodium thiocyanate, 0.3-0.6 parts air-entraining agent, 6-8 parts modified nano titanium dioxide, and 8-10 parts ternary phase change material. This nanocomposite phase change antifreeze water-reducing agent is a composite functional admixture that introduces nanomaterials and phase change materials into traditional antifreeze water-reducing agents. It not only prevents concrete from freezing at low temperatures but also regulates the internal temperature changes of concrete through "phase change" characteristics, thereby improving the durability of concrete under freeze-thaw cycles.

The application discloses a preparation method of carbon sphere loaded small-size platinum group metal nanoparticles. The method comprises the following steps: adding a dopamine hydrochloride solution into a mixed solution of ethanol, water and ammonia water, stirring and reacting to prepare polydopamine microspheres, adding a ruthenium ion salt and a platinum group metal ion salt, stirring to enable the polydopamine microspheres to fully adsorb the ruthenium ion and the platinum group metal ion, and finally calcining the polydopamine microspheres with the adsorbed metal ions in an inert atmosphere at high temperature to prepare the carbon sphere loaded small-size platinum group metal nanoparticles. The carbon sphere loaded platinum group metal nanoparticles prepared by the method have small size, uniform distribution and an average particle size of 2-3 nm. The method is simple, suitable for preparation of various small-size platinum group metal nanoparticle materials and easy for large-scale production.