The application discloses a kind of
synthesis methods of high-purity 2-bromo-6-nitrobenzaldehyde, belong to
organic synthesis technical field, the synthesis method is at 20-30 ℃, 1,2-
dichloroethane, 2-bromo-6-nitrotoluene is mixed, stirring is dissolved, N-
bromine phthalimide and initiator are mixed, heating to 70-100 ℃,
reflux reaction, cooling to 20-30 ℃, post-
processing is obtained
compound A;
Compound A is mixed with
acetonitrile,
temperature control is 0-10 ℃, batch is added urotropine, stirring is at 20-40 ℃,
acetic acid is added, stirring is at 70-100 ℃, post-
processing is obtained 2-bromo-6-nitrobenzaldehyde;The synthesis method of the application can solve the problems of low product yield, low purity,
poor quality, serious three waste
pollution, high cost and difficult industrialization existing in the prior art of 2-bromo-6-nitrobenzaldehyde synthesis method.