Antibacterial and antistatic fiber coating and preparation method thereof
A technology of antistatic fiber and antistatic fiber, which is applied in fiber processing, biochemical fiber processing, textiles and papermaking, etc.
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Embodiment 1
[0040] An antibacterial and antistatic fiber coating and a preparation method thereof mainly include, by weight parts: 2 parts of modified carboxymethyl chitosan quaternary ammonium salt, and 16 parts of aminated modified graphene.
[0041] A kind of preparation method of antibacterial antistatic fiber coating, the preparation method of described antibacterial antistatic fiber coating mainly comprises following preparation steps:
[0042] (1) Carboxymethyl chitosan is added in the three-neck flask with stirring and reflux device, and 40% hydrogen oxidation of 7 times of carboxymethyl chitosan quality isopropanol and carboxymethyl chitosan quality 1 time is added Sodium aqueous solution, stirred and heated in a water bath to raise the temperature of the material to 45.0 ° C, and continued to stir for 1 hour to alkalinize the mixed solution; then slowly added 40% 3-chloro -2 hydroxypropyltrimethylammonium chloride solution, control the titration time at 1h; after reacting for 8h...
Embodiment 2
[0053] An antibacterial and antistatic fiber coating and a preparation method thereof mainly include, by weight parts: 2 parts of carboxymethyl chitosan quaternary ammonium salt, and 16 parts of aminated modified graphene.
[0054] A kind of preparation method of antibacterial antistatic fiber coating, the preparation method of described antibacterial antistatic fiber coating mainly comprises following preparation steps:
[0055] (1) Carboxymethyl chitosan is added in the three-neck flask with stirring and reflux device, and 40% hydrogen oxidation of 7 times of carboxymethyl chitosan quality isopropanol and carboxymethyl chitosan quality 1 time is added Sodium aqueous solution, stirred and heated in a water bath to raise the temperature of the material to 45.0 ° C, and continued to stir for 1 hour to alkalinize the mixed solution; then slowly added 40% 3-chloro -2 hydroxypropyltrimethylammonium chloride solution, control the titration time at 1h; after reacting for 8h, adjust ...
Embodiment 3
[0064] An antibacterial and antistatic fiber coating and a preparation method thereof, mainly comprising: 2 parts of modified carboxymethyl chitosan quaternary ammonium salt and 16 parts of graphene oxide in parts by weight.
[0065] A kind of preparation method of antibacterial antistatic fiber coating, the preparation method of described antibacterial antistatic fiber coating mainly comprises following preparation steps:
[0066] (1) Carboxymethyl chitosan is added in the three-neck flask with stirring and reflux device, and 40% hydrogen oxidation of 7 times of carboxymethyl chitosan quality isopropanol and carboxymethyl chitosan quality 1 time is added Sodium aqueous solution, stirred and heated in a water bath to raise the temperature of the material to 45.0 ° C, and continued to stir for 1 hour to alkalinize the mixed solution; then slowly added 40% 3-chloro -2 hydroxypropyltrimethylammonium chloride solution, control the titration time at 1h; after reacting for 8h, adjus...
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