Heat-conducting material and preparation process thereof
A technology of heat-conducting materials and inhibitors, applied in the direction of heat exchange materials, coatings, chemical instruments and methods, etc., can solve the problems of poor thermal conductivity of silica gel pads, limited application range, insufficient heat conduction channels, etc., to facilitate calendering processing, Improve the effect of stretching and tearing, good heat soaking function
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[0038] Further, the preparation method of the modified alumina particles comprises the following steps:
[0039] S21, put hexamethyldisilazane into propanol, stir and mix with an electromagnetic stirrer, the stirring speed is 300r / min-450r / min, and the stirring time is 30min, and prepare a mixed solution;
[0040] S22, adding spherical alumina particles into the mixed solution, and obtaining modified spherical alumina particles after stirring and drying.
[0041] Further, the rotation speed of the agitator in S2 is 3500r / min-4000r / min, the stirring time is 15min-30min, the high-temperature vulcanization molding temperature is 155°C-175°C, and the vulcanization time is 60min-80min.
[0042] Further, the initial kneading temperature of the vacuum kneader in S2 is 95°C-100°C, the initial kneading time is 100min-120min, the secondary kneading temperature of the vacuum kneader is 120°C-130°C, and the secondary kneading time is 50min-60min .
[0043] Further, the hot air vulcaniza...
Embodiment example 1
[0047] Weigh 45 parts of hexamethyldisilazane, 100 parts of methanol and 700 parts of alumina particles, put hexamethyldisilazane into propanol, stir and mix with an electromagnetic stirrer, the stirring speed is 450r / min, The stirring time is 30min, and it is configured into a mixed solution, and then spherical alumina particles are added to the mixed solution. After stirring and drying, the stirring time is 1h, and the drying is carried out twice. When drying for the first time, the drying temperature is 120°C, the time is 1.5h, during the second drying, the temperature is 160°C, the time is 0.5h, and the modified spherical alumina particles are obtained;
[0048] Weigh 100 parts of methyl vinyl silicone oil, 15 parts of hydrogen-containing silicone oil, 300 parts of modified alumina particles, 50 parts of graphene fiber powder, 90 parts of propanol solution, 5 parts of coupling agent, 8 parts of catalyst, inhibitor 9 parts, 15 parts of cross-linking agent, 20 parts of antio...
Embodiment example 2
[0052] Weigh 45 parts of hexamethyldisilazane, 100 parts of methanol and 700 parts of alumina particles, put hexamethyldisilazane into propanol, stir and mix with an electromagnetic stirrer, the stirring speed is 450r / min, The stirring time is 30min, and it is configured into a mixed solution, and then spherical alumina particles are added to the mixed solution. After stirring and drying, the stirring time is 1h, and the drying is carried out twice. When drying for the first time, the drying temperature is 120°C, the time is 1.5h, during the second drying, the temperature is 160°C, the time is 0.5h, and the modified spherical alumina particles are obtained;
[0053] Weigh 130 parts of methyl vinyl silicone oil, 25 parts of hydrogen-containing silicone oil, 400 parts of modified alumina particles, 75 parts of graphene fiber powder, 90 parts of propanol solution, 5 parts of coupling agent, 8 parts of catalyst, inhibitor 9 parts, 15 parts of cross-linking agent, 20 parts of antio...
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