Phosphate near-infrared luminescent temperature measurement material and preparation method thereof
A phosphate and near-infrared technology, used in luminescent materials, chemical instruments and methods, etc., can solve problems such as damage to samples and temperature changes, and achieve the effects of stable chemical properties, easy grinding, and high photoconversion efficiency.
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Embodiment 1
[0032] The raw material is SrCO 3 (analytical pure), Li 2 CO 3 (analytical pure), Cr 2 o 3 (99.99%) and NH 4 h 2 PO 4(Analytical pure), the molar ratio between them is 1.994:0.0015:0.0015:2, weigh the raw materials according to the above ratio, mix them and place them in a corundum crucible, pre-fire at 600°C for 5 hours, and cool to room temperature Grind it again, put it into a high-temperature furnace, bake it at 1100°C for 3 hours in a CO atmosphere, and cool it down to room temperature naturally to obtain a luminescent temperature-measuring powder. The obtained luminescent temperature measuring powder is a white powder with a molecular formula of Sr 1.994 Li 0.003 P 2 o 7 :0.003Cr 3+ , under the excitation of 488nm blue light, its emission spectrum consists of a broadband emission with a main peak at 840nm and a half-maximum width of 140nm, such as figure 1 As shown; with the increase of temperature, the peak intensity decreased sharply, as figure 2 Shown; T...
Embodiment 2
[0034] The raw material is SrCO 3 (analytical pure), Li 2 CO 3 (analytical pure), Cr 2 o 3 (99.99%) and NH 4 h 2 PO 4 (Analytical pure), the molar ratio between them is 1.994:0.0015:0.0015:2, weigh the raw materials according to the above ratio, mix them and place them in a corundum crucible, pre-fire at 700°C for 5 hours, and cool to room temperature Grind it again, put it into a high-temperature furnace, bake it at 1100°C for 3 hours in a CO atmosphere, and cool it down to room temperature naturally to obtain a luminescent temperature-measuring powder. The obtained luminescent temperature measuring powder is a white powder with a molecular formula of Sr 1.994 Li 0.003 P 2 o 7 :0.003Cr 3+ , under the excitation of 488nm blue light, its emission spectrum consists of a broadband emission with a main peak at 840nm and a half-maximum width of 140nm. The peak intensity decreased sharply with increasing temperature. The integral area of the emission peak changes line...
Embodiment 3
[0036] The raw material is SrCO 3 (analytical pure), Li 2 CO 3 (analytical pure), Cr 2 o 3 (99.99%) and NH 4 h 2 PO 4 (analytical pure), the molar ratio between them is 1.994:0.0015:0.0015:2, weigh the raw materials according to the above ratio, mix them and place them in a corundum crucible, pre-fire at 900°C for 5 hours, and cool to room temperature Grind it again, put it into a high-temperature furnace, bake it at 1100°C for 3 hours in a CO atmosphere, and cool it down to room temperature naturally to obtain a luminescent temperature-measuring powder. The obtained luminescent temperature measuring powder is a white powder with a molecular formula of Sr 1.994 Li 0.003 P 2 o 7 :0.003Cr 3+ , under the excitation of 488nm blue light, its emission spectrum consists of a broadband emission with a main peak at 840nm and a half-maximum width of 140nm. The peak intensity decreased sharply with increasing temperature. The integral area of the emission peak changes line...
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