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Treatment method for regenerating and recovering sulfuric acid from recovered waste acid of lead-acid battery

A lead-acid battery and treatment method technology, applied in electrochemical water/sewage treatment, water/sewage treatment, heated water/sewage treatment, etc., can solve problems such as high cost and waste of resources, improve recovery rate and reduce resources Waste, the effect of improving recycling efficiency

Inactive Publication Date: 2021-12-10
太和县大华能源科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] Aiming at the deficiencies of the prior art, the present invention provides a treatment method for regenerating and recovering sulfuric acid from lead-acid battery recovery waste acid, which solves the existing cost of regenerating sulfuric acid from lead-acid battery recovery waste acid in the prior art High, waste of resources

Method used

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  • Treatment method for regenerating and recovering sulfuric acid from recovered waste acid of lead-acid battery
  • Treatment method for regenerating and recovering sulfuric acid from recovered waste acid of lead-acid battery
  • Treatment method for regenerating and recovering sulfuric acid from recovered waste acid of lead-acid battery

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Effect test

Embodiment 1

[0038] see Figure 1-9 Shown, a kind of processing method of regenerating and reclaiming sulfuric acid from lead-acid battery recycling waste acid, specifically comprises the following steps:

[0039] Step 1, send the waste polluted acid recovered from the lead-acid battery into the recovery box 10 through the feed pipe 107, connect the positive and negative poles of the power supply to the electrode assemblies at the front and back of the recovery box 10, and utilize the lead recovery plate 102 of the power supply to The lead in the waste sewage acid is reclaimed, and the lead in the waste sewage acid is adsorbed on the surface of the lead recovery plate 102, and the waste sewage acid processed through the lead recovery process inside the recovery box 10 is pumped into the preheating box 20 by the material pump 109;

[0040] Step 2, the waste acid enters the inside of the retort 401 through the feed pipe 302, and the heater 403 inside the heating frame 402 is used to heat the...

Embodiment 2

[0045] see Figure 1-9 As shown, in the present invention, the equipment used for regenerating and reclaiming sulfuric acid from lead-acid battery recycling waste acid includes recovery box 10, preheating box 20, distillation box 30 and treatment box 40, preheating box 20, distillation box 30 and treatment box 40 is located on one side of the recovery box 10, and the interior of the recovery box 10 is provided with a recovery mechanism, and the recovery mechanism includes a connecting frame 101 and several lead recovery plates 102 located at the bottom of the connecting frame 101, and both sides of the recovery box 10 inner wall are provided with The chute 103 matched with the connecting frame 101, and the both sides of the connecting frame 101 are respectively connected with the inside sliding of the two chute 103, the front and rear sides of the recovery box 10 inside are all provided with a movable frame 104, the two movable frames 104 Two servo electric cylinders 105 are a...

Embodiment 3

[0049] In the present invention, the inside of the preheating box 20 is provided with a heat exchange sleeve 301 and a material guide tube 302 located inside the heat exchange sleeve 301, and a heat exchange is formed between the surface of the material guide tube 302 and the inside of the heat exchange sleeve 301. Runner 303, using heat exchange runner 303 to realize the preheating treatment of waste acid in feed pipe 302, and then improve the treatment efficiency of waste acid inside distillation tank 401, the left end of feed pipe 302 is connected with the feed pump 109 The discharge end is connected, and the right end of the material guide pipe 302 runs through the preheating box 20 and extends to the outside of the preheating box 20. The upper and lower sides of the right side of the preheating box 20 are respectively provided with an air inlet pipe 304 and an air outlet pipe 305. Through the air inlet pipe 304 and outlet pipe 305 realize the recycling of the steam generat...

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Abstract

The invention relates to the technical field of chemical resource regeneration and recovery, in particular to a treatment method for regenerating and recovering sulfuric acid from waste acid recovered from a lead-acid battery, which comprises the following steps: recovering lead-containing substances in the waste acid, preheating the waste acid, distilling the waste acid, and finally treating waste gas and waste liquid. According to the treatment method, waste acid is firstly introduced into a recycling box, and a lead recycling plate in the recycling box is used for recycling substances in the waste acid, so that on one hand, the waste of resources in the waste acid is reduced, on the other hand, the recycling efficiency of sulfuric acid in the waste acid is improved, and the influence of other substances in the waste acid on the recycling of the sulfuric acid is avoided; and meanwhile, the recovery rate of sulfuric acid in the waste acid is further improved. According to the invention, an electrode assembly is arranged in the recycling box, and the electrode assembly is movably connected with a connecting frame, so that the connecting frame is flexibly assembled in the recycling box, and then substances adsorbed on the lead recycling plate are conveniently collected.

Description

technical field [0001] The invention relates to the technical field of regeneration and recovery of chemical resources, in particular to a treatment method for regeneration and recovery of sulfuric acid from waste acid recovered from lead-acid batteries. Background technique [0002] With the rapid development of the automobile industry, used up waste batteries contain a large amount of heavy metals and electrolytes. Whether buried deep or stacked in the open, the heavy metals and electrolytes in them will pollute groundwater, soil and the surrounding environment, endangering human health. However, waste batteries are also valuable secondary resources that can be utilized by human beings, so the comprehensive utilization of waste batteries is of great significance. [0003] Publication number is the invention patent in CN111994878A and has proposed a kind of method that regenerates and reclaims sulfuric acid from waste acid of lead-acid battery recovery, and this invention p...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C02F9/10B01D53/18C02F1/66C01B17/90C01B17/88
CPCC02F9/00B01D53/1418B01D53/1456B01D53/185C02F1/66C01B17/901C01B17/88C01B17/90C02F1/043C02F1/46C02F1/02C02F2209/19
Inventor 毛荣海刘俊杰朱乾龙杜文明刘坤明
Owner 太和县大华能源科技有限公司