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Method for synchronously extracting mustard essential oil and mustard oil and mustard seed extract

A mustard essential oil and simultaneous extraction technology, applied in the field of mustard seed extract, simultaneous extraction of mustard essential oil and mustard oil, can solve the problems of consuming manpower, material resources and financial resources, difficult to control production quality, lengthy production process, etc., and achieve less waste in the process , the effect of high extraction rate and low process cost

Pending Publication Date: 2021-12-24
NANYANG ZHANGZHONGJING SUPER KITCHEN
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Throughout the production process, the production process is lengthy and incoherent, which consumes a lot of manpower, material and financial resources; materials are transferred between different equipments many times, making it difficult to control the production quality and potential safety risks

Method used

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  • Method for synchronously extracting mustard essential oil and mustard oil and mustard seed extract
  • Method for synchronously extracting mustard essential oil and mustard oil and mustard seed extract
  • Method for synchronously extracting mustard essential oil and mustard oil and mustard seed extract

Examples

Experimental program
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Effect test

Embodiment 1

[0051] In this embodiment, black mustard seeds are used as raw materials to prepare mustard essential oil and mustard oil, and the specific methods are as follows:

[0052] S1, 100kg of black mustard seeds are fried and pulverized, and sieved through a 40-mesh sieve.

[0053] S2. Mix myrosinase with an activity unit of 200UN and water at a mass ratio of 0.5:100, and adjust the pH of the enzyme to 6.0 with glacial acetic acid.

[0054] S3. The black mustard seed powder and the myrosinase solution are mixed according to the mass ratio of 1.0:0.5, then put into the extraction kettle of a supercritical extraction device, and enzymatically hydrolyzed at 55° C. for 1 hour.

[0055] S4. Turn on the supercritical extraction equipment, set the extraction pressure to 20Mpa, the temperature to 35°C, and the flow rate of carbon dioxide to 50L / min, to start the extraction operation, and stop the extraction operation after 4 hours.

[0056] S5. Open the valve at the bottom of the analytica...

Embodiment 2

[0061] In this embodiment, yellow mustard seeds are used as raw materials to prepare mustard essential oil and mustard oil, and the specific methods are as follows:

[0062] S1, 100kg of yellow mustard seeds are fried and pulverized, and sieved through a 40-mesh sieve.

[0063] S2, myrosinase and water were mixed evenly at a mass ratio of 0.3:100, and the pH of the enzyme was adjusted to 6.0 with glacial acetic acid.

[0064] S3. The yellow mustard seed powder and the myrosinase solution are mixed according to the mass ratio of 1.0:0.3, then put into a supercritical extraction kettle, and enzymatically hydrolyzed at 55°C for 0.5h.

[0065] S4. Turn on the supercritical extraction equipment, set the extraction pressure to 20Mpa, the temperature to 35°C, and the flow rate of carbon dioxide to 50L / min, to start the extraction operation, and stop the extraction operation after 3 hours.

[0066] S5. Open the valve at the bottom of the analytical kettle, pump the collected oil into...

Embodiment 3

[0071] In this embodiment, yellow mustard seeds are used as raw materials to prepare mustard essential oil and mustard oil, and the specific methods are as follows:

[0072] S1, 100kg of yellow mustard seeds are fried and pulverized, and sieved through a 60-mesh sieve.

[0073] S2, myrosinase and water were mixed evenly at a mass ratio of 1:100, and the pH of the enzyme was adjusted to 5.0 with glacial acetic acid.

[0074] S3. The yellow mustard seed powder and myrosinase solution were mixed according to the mass ratio of 1.0:1.5, then put into a supercritical extraction kettle, and enzymatically hydrolyzed at 55° C. for 2 hours.

[0075] S4. Turn on the supercritical extraction equipment, set the extraction pressure to 25Mpa, the temperature to 35°C, and the flow rate of carbon dioxide to 40L / min, to start the extraction operation, and stop the extraction operation after 4 hours.

[0076] S5. Open the valve at the bottom of the analytical kettle, pump the collected oil into...

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Abstract

The invention discloses a method for synchronously extracting mustard essential oil and mustard oil and a mustard seed extract, and relates to the technical field of deep processing of agricultural products. The method comprises the following steps: carrying out supercritical extraction on enzymolysis mustard seed powder to obtain extract liquor, and carrying out vacuum purifying on the extract liquor to obtain a mixture of mustard essential oil and mustard oil. According to the method for synchronously extracting the mustard essential oil and the mustard oil, the process route is simple, extraction and purifying of the mustard essential oil and the mustard oil are completed at a time, and the process cost is low; the target component extraction rate is high, the mustard essential oil extraction rate reaches 80% or above, and the mustard oil extraction rate reaches 85% or above; and the requirements of national safe food production are met, the waste amount in the process is small, and the current green food industry development trend is met.

Description

technical field [0001] The invention relates to the technical field of deep processing of agricultural products, in particular to a method for synchronously extracting mustard essential oil and mustard oil and mustard seed extract. Background technique [0002] Mustard seed is the seed of the cruciferous plant mustard, containing 20-40% oil and 2-4% sinaprin (glucosinolate). Myrosinin can be produced under the catalyzed hydrolysis of myrosinase (also known as glucosinolate glucohydrolase, glucosidase, thioglucoside, CAS9025-38-1, EC3.2.1.147), which has a unique irritating and spicy flavor Mustard essential oil (isothiocyanate substances) is used as a food seasoning. It has the characteristics of relieving greasy and refreshing taste and increasing appetite. At the same time, it has certain insecticidal, bactericidal and antiseptic functions. favored. It is of great significance to fully extract mustard essential oil and mustard oil contained in mustard seeds, and a large ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B1/02C11B1/04C11B1/10C11B9/02A23L27/10
CPCC11B1/025C11B1/04C11B1/104C11B9/025A23L27/11A23V2002/00A23V2200/16A23V2250/21
Inventor 李正纪郭欣薄晓菲
Owner NANYANG ZHANGZHONGJING SUPER KITCHEN