High-voltage positive electrode material of liquid or semi-liquid metal battery and application thereof
A positive electrode material and metal battery technology, applied in the direction of battery electrodes, circuits, electrical components, etc., can solve the problems of low energy density, low working voltage, etc., and achieve the goal of increasing specific capacity and energy density, increasing discharge voltage, and improving Coulombic efficiency Effect
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Embodiment 1
[0043] In this embodiment, a selenium-bismuth alloy is used as the positive electrode material, and the mole percentage of selenium and bismuth is 20:80 mol%. Lithium metal is the negative electrode material. The electrolyte is a binary molten salt composed of LiCl and KCl, wherein the molar percentage of LiCl and KCl is 59:41 mol%.
[0044] The preparation process of the selenium-bismuth alloy used in this example is as follows: Weigh 0.81 g of selenium and 8.57 g of bismuth with an electronic balance, mix them mechanically and put them into a graphite crucible, heat the crucible to 550°C under the protection of an inert atmosphere and keep it warm for 10 hours to make the raw materials Fully alloyed, the positive electrode material Se can be obtained after cooling down 20 Bi 80 .
[0045] In this embodiment, a porous foam nickel-iron alloy is selected as the negative electrode current collector, which is immersed in molten metal lithium to absorb 0.14 g of liquid metal li...
Embodiment 2
[0049] In this embodiment, a selenium-bismuth alloy is used as the positive electrode material, and the mole percentage of selenium and bismuth is 30:70 mol%. Lithium metal is the negative electrode material. The electrolyte is a binary molten salt composed of LiCl and KCl, wherein the molar percentage of LiCl and KCl is 59:41 mol%.
[0050] The preparation process of the selenium-bismuth alloy used in this example is as follows: Weigh 0.81 g of selenium and 5.00 g of bismuth with an electronic balance, mix them mechanically and put them into a graphite crucible, heat the crucible to 550° C. under the protection of an inert atmosphere and keep it warm for 10 hours to make the raw materials Fully alloyed, the positive electrode material Se can be obtained after cooling down 30 Bi 70 .
[0051] In this embodiment, a porous foam nickel-iron alloy is selected as the negative electrode current collector, which is immersed in molten metal lithium to absorb 0.14 g of liquid metal ...
Embodiment 3
[0055] In this embodiment, a selenium-bismuth alloy is used as the positive electrode material, and the mole percentage of selenium and bismuth is 40:60 mol%. Lithium metal is the negative electrode material. The electrolyte is a ternary molten salt composed of LiF, LiCl and LiBr, wherein the molar percentage of LiF, LiCl and LiBr is 22:31:47 mol%.
[0056]The preparation process of the selenium-bismuth alloy used in this example is as follows: weigh 0.81 g of selenium and 3.22 g of bismuth with an electronic balance, put them into a graphite crucible after mechanical mixing, heat the crucible to 550 ° C under the protection of an inert atmosphere and keep it warm for 10 hours to make the raw materials Fully alloyed, the positive electrode material Se can be obtained after cooling down 40 Bi 60 .
[0057] In this embodiment, a porous foam nickel-iron alloy is selected as the negative electrode current collector, which is immersed in molten metal lithium to absorb 0.14 g of ...
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