Method for synthesizing titanium-aluminum binary oxide catalyst by sol-gel method
A binary oxide, sol-gel technology, applied in physical/chemical process catalysts, chemical instruments and methods, chemical/physical processes, etc., can solve the problems of low catalytic efficiency, complex catalyst synthesis, high cost, and achieve high Catalytic efficiency, the effect of improving catalytic efficiency and low production cost
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0041] 1) Dissolve 0.8 g of PVP in 30 ml of distilled water, and add Ti (OBU) according to 1: 1 molar ratio. 4 And Al (no 3 ) 3 · 9h 2 O, stir it for 5 min, then add 2.5 mmol nabh 4 , Stirred at 25 ° C for 2 h;
[0042] 2) Transfer the above mixture to the reactor, 100 ° C reaction for 24 hours, then naturally cooled to obtain a mixture;
[0043] 3) Collecting the above mixed liquid, washed with ethanol (3 × 3 mL) and distilled water (3 × 3 mL), dried in air at 60 ° C for 12 h, to give a titanium-aluminum diazo-aluminum di-aluminum-aluminum oxide white solid powder 0.13g, remembered C1.
Embodiment 2
[0045] 1) Dissolve 0.8 g of PVP in 30 ml of distilled water, and add Ti (OBU) according to 1: 1 molar ratio. 4 And Al (no 3 ) 3 · 9h 2 O, stir it for 5 minutes, then add 2.5mmol NH 3 · H 2 O, stirred at 25 ° C for 2 h;
[0046] 2) Transfer the above mixture to the reactor, 100 ° C reaction for 24 hours, then naturally cooled to obtain a mixture;
[0047] 3) Collecting the above mixture, washed with ethanol (3 × 3 mL) and distilled water (3 × 3 mL), dried in air at 60 ° C for 12 h, to give a titanium-aluminum diazo-aluminum oxide white solid powder 0.11g, recorded C2.
Embodiment 3
[0049] 1) Take 30ml distilled water, and add Ti (OBU) to the molar ratio of 1: 1. 4 And Al (no 3 ) 3 · 9h 2 O, stir it for 5 minutes, then add 2.5mmol NH 3 · H 2 O, stirred at 25 ° C for 2 h;
[0050] 2) Transfer the above mixture to the reactor, 100 ° C reaction for 24 hours, then naturally cooled to obtain a mixture;
[0051] 3) The above mixture was centrifuged, washed with ethanol (3 × 3 mL) and distilled water (3 × 3 mL), dried in air at 60 ° C for 12 h to give a titanium-aluminum diazo oxide white solid powder 0.10g, remembered C3.
PUM
Login to view more Abstract
Description
Claims
Application Information
Login to view more - R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap