Production process of durable photochromic PET (Polyethylene Terephthalate) film
A technology of photochromism and production technology, which is applied in the field of material science, can solve the problems of unsuitable polyester film production line, unsuitable for large-scale production, and unable to be used in factories, so as to achieve excellent optical performance and avoid uneven and uniform optical performance The effect of strong adhesion
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[0038] (1) Preparation of photochromic sol solution
[0039] Step 1: WO 3 Preparation of sol: add Na to ultrapure water 2 WO 4 2H 2 O, stir to dissolve, and add mineral acid solution to acidify to PH=4 to obtain WO 3 solution. adding oxalic acid into the ultrapure water to dissolve, and heating and stirring during the dissolution process to obtain an oxalic acid solution. The heating temperature is 45-63°C, and the stirring time is 5-10min. WO 3 solution and oxalic acid solution, and add ultrapure water to dilute and stir, after standing for 6-10h, a colorless and transparent WO 3 Sol, the concentration is 0.3M.
[0040] Step 2: TiO 2 Sol preparation: the C 16 h 36 o 4 Ti (butyl titanate) was added to absolute ethanol, and then ultrapure water was added to the solution for polycondensation reaction to prepare TiO with a sol concentration of 0.3 M 2 Sol.
[0041] Step 3: Preparation of ZnO sol: (CH 3 COO) 2 Zn·2H 2 O was dissolved in anhydrous ethanol solution ...
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