Anti-SARS-CoV-2 neutralizing antibody and application thereof
A sars-cov-2, antibody technology, applied in the direction of antibodies, applications, antiviral agents, etc., to achieve the effect of high-efficiency neutralization activity
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Embodiment 1
[0090] Example 1. Screening of anti-SARS-CoV-2 neutralizing antibodies
[0091] (1) Plasma neutralization activity detection
[0092] 1. Sample: Plasma of volunteers immunized twice with the novel coronavirus inactivated vaccine (BBIBP-CorV).
[0093] 2. Neutralization activity detection: Detect the neutralization of 28 samples against SARS-CoV-2 wild type and mutant strains (Alpha, Betav1, Beta v2, Beta v3, Gamma, Delta, Lambda, Kappa, Epsilon, Zeta) pseudoviruses Titer. Methods as below:
[0094] (1) Plasma samples (named plasma No. 1-No. 28) were heat-inactivated at 56°C for 30 min, and centrifuged briefly to remove insoluble matter.
[0095] (2) In a 96-well cell culture plate, add 150 µl GM (DEME+10%FBS+1% double antibody) to the cell control (column 1), add 100 µl GM to the remaining wells, and add another 30 µl GM to 3A- 3H and 8A-8H (1-12 is column 1-12, A-H is row A-H, for example, 3A is the treatment well of column 3 and row A in a 96-well plate).
[0096] (3) T...
Embodiment 2
[0181] Example 2. Preparation of neutralizing antibodies
[0182] (1) Primary screening of antibody activity
[0183] 1. Antibody expression in 293T cell system
[0184] Transiently transfect the successfully paired antibody heavy chain and light chain gene expression vectors into 293T cells:
[0185] (1) 24 hours before transfection in a 12-well plate, each well was plated with 5×10 5 293T cells.
[0186] (2) On the day of transfection, observe the confluence of the cells, preferably 70%-80%.
[0187] (3) Take 1 μg of the plasmid DNA extracted by the plasmid mini-extraction kit (Tiangen, DP103) and dilute it with 60 μl of Opti-MEM medium.
[0188] (4) Dilute 4 μl Lipofectamine® 2000 Reagent with 60 μl Opti-MEM medium.
[0189] (5) Mix the above-mentioned diluted DNA and Lipofectamine® 2000 at a volume of 1:1 to obtain a mixture, and incubate at room temperature for 5 min.
[0190] (6) Take 120 μl of the mixture and gently add it to 293T cells in 5% CO 2 Incubate at 37...
Embodiment 3
[0235] Example 3. Antibody 6-2C affinity and neutralizing activity analysis
[0236] The neutralizing antibody 6-2C prepared in Example 2 was used to carry out the following experiments.
[0237] (1) Affinity analysis of neutralizing antibodies
[0238] 1. BLI detection of the binding ability of neutralizing antibody 6-2C to SARS-CoV-2 RBD
[0239] (1) Ligand coupling: In the high-throughput molecular interaction instrument Octet RED 384, biotin-labeled 10 µg / ml RBD protein (Acrobiosystems, SPD-C82E9) was coupled to the SA sensor (SARTORIUS, 18-0009) superior.
[0240] (2) Antibody 6-2C was serially diluted 2-fold with PBS starting from 320 nM for 6 gradients.
[0241] (3) According to the table 4 below, set the injection analysis from low concentration to high concentration.
[0242]
[0243] (4) Data analysis: set the following table 5 in the analysis software, and perform curve fitting.
[0244]
[0245] 2. Analysis of the results: the affinity Kd between 6-2C an...
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