Preparation method of large biological functional agent containing active ingredients of navel oranges
A technology of active ingredients and functional agents, which is applied in the field of preparation of large biological functional agents, can solve the problems of poor fatliquor filling, poor leather strength, and reduce leather haze, so as to improve tear strength, tensile strength, and The effect of antimicrobial properties
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Examples
Embodiment 1
[0041] (1) Preparation of modified palm oil
[0042] Mix palm oil with p-tert-butylphenyl glycidyl ether, add dicyclohexyl peroxydicarbonate, heat up to 70°C under nitrogen protection and stir for 150min to obtain preliminary modified palm oil, and mix hydrogen-containing silicone oil with preliminary modified palm oil. mixed with palm oil, heated to 65℃, stirred at -0.05Mpa for 30min, then added Raney nickel catalyst, heated to 75℃, stirred for 90min, removed the catalyst to obtain modified palm oil;
[0043] Described palm oil is 58 degree palm oil;
[0044] The mass ratio of described palm oil and p-tert-butylphenyl glycidyl ether is 3:2;
[0045] The mass ratio of described dicyclohexyl peroxydicarbonate and palm oil is 1:50;
[0046] The hydrogen content of the hydrogen-containing silicone oil is 0.15%;
[0047] The mass ratio of the hydrogen-containing silicone oil to the preliminary modified palm oil is 1:3;
[0048] The nickel content of the Raney nickel catalyst i...
Embodiment 2
[0075] (1) Preparation of modified palm oil
[0076] Mix palm oil with p-tert-butylphenyl glycidyl ether, add dicyclohexyl peroxydicarbonate, heat up to 65°C under nitrogen protection and stir for 180min to obtain preliminary modified palm oil, mix hydrogen-containing silicone oil with preliminary modified palm oil. mixed with palm oil, heated to 60℃, stirred at -0.04Mpa for 40min, then added Raney nickel catalyst, heated to 70℃, stirred for 100min, removed the catalyst to obtain modified palm oil;
[0077] Described palm oil is 58 degree palm oil;
[0078] The mass ratio of described palm oil and p-tert-butylphenyl glycidyl ether is 2.5:2;
[0079] The mass ratio of described dicyclohexyl peroxydicarbonate and palm oil is 1:40;
[0080] The hydrogen content of the hydrogen-containing silicone oil is 0.12%;
[0081] The mass ratio of the hydrogen-containing silicone oil to the preliminary modified palm oil is 1:2.5;
Embodiment 3
[0109] (1) Preparation of modified palm oil
[0110] Mix palm oil with p-tert-butylphenyl glycidyl ether, add dicyclohexyl peroxydicarbonate, heat up to 75°C under nitrogen protection and stir for 130min to obtain preliminary modified palm oil, mix hydrogen-containing silicone oil with preliminary modified palm oil. mixed with palm oil, heated to 70°C, stirred at -0.06Mpa for 25min, then added Raney nickel catalyst, heated to 80°C and stirred for 80min, removed the catalyst to obtain modified palm oil;
[0111] Described palm oil is 58 degree palm oil;
[0112] The mass ratio of described palm oil and p-tert-butylphenyl glycidyl ether is 3.5:2;
[0113] The mass ratio of described dicyclohexyl peroxydicarbonate and palm oil is 1:60;
[0114] The hydrogen content of the hydrogen-containing silicone oil is 0.17%;
[0115] The mass ratio of the hydrogen-containing silicone oil to the preliminary modified palm oil is 1:3.5;
[0116] The nickel content of the Raney nickel catal...
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Abstract
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