Cast-rolled aluminum foil for aseptic packaging and preparation method of cast-rolled aluminum foil
A packaging, casting and rolling technology, applied in coating, metal material coating process, etc., can solve the problems of insufficient antibacterial performance and low output of double-zero aluminum foil.
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Embodiment 1
[0045] The present embodiment is a preparation method of an antibacterial agent, comprising the following steps:
[0046] A1: Add 1.0g cyanuric acid, 0.43g potassium hydroxide and 100mL deionized water into a three-necked flask equipped with a stirrer and a thermometer, and stir the reaction at a temperature of 75°C and a stirring rate of 300r / min After 2 hours, 20 mmol of 4,6-dibromoindole was added and the reaction was continued for 8 hours. After the reaction, the reaction product was centrifuged, and the precipitate was washed twice with distilled water, and then placed in a vacuum drying box and dried to constant weight to obtain an intermediate body 1;
[0047] A2: Add 10 mmol of p-bromoiodobenzene and 20 mL of tetrahydrofuran to a three-necked flask equipped with a stirrer, a thermometer, a gas pipe and a constant pressure dropping funnel, pass into argon protection, at a temperature of -78°C, and at a stirring rate of 100r Stir under the condition of / min for 30min, t...
Embodiment 2
[0052] The present embodiment is a preparation method of an antibacterial agent, comprising the following steps:
[0053] A1: Add 1.0g cyanuric acid, 0.43g potassium hydroxide and 100mL deionized water into a three-necked flask equipped with a stirrer and a thermometer, and stir the reaction at a temperature of 78°C and a stirring rate of 400r / min After 2.5h, 25mmol of 4,6-dibromoindole was added and the reaction was continued for 9h. After the reaction, the reaction product was centrifuged, and the precipitate was washed three times with distilled water, and then placed in a vacuum drying box and dried to constant weight to obtain Intermediate 1;
[0054] A2: Add 10 mmol of p-bromoiodobenzene and 25 mL of tetrahydrofuran to a three-necked flask equipped with a stirrer, a thermometer, a gas pipe and a constant pressure dropping funnel, and pass through argon protection. The temperature is -78°C, and the stirring rate is 150r. Stir under the condition of / min for 35min, then a...
Embodiment 3
[0059] The present embodiment is a preparation method of an antibacterial agent, comprising the following steps:
[0060] A1: Add 1.0 g of cyanuric acid, 0.43 g of potassium hydroxide and 100 mL of deionized water into a three-necked flask equipped with a stirrer and a thermometer, and stir the reaction at a temperature of 80°C and a stirring rate of 500 r / min. After 3h, 30mmol of 4,6-dibromoindole was added and the reaction was continued for 10h. After the reaction, the reaction product was centrifuged, and the precipitate was washed three times with distilled water, and then placed in a vacuum drying box and dried to constant weight to obtain an intermediate body 1;
[0061] A2: Add 10 mmol of p-bromoiodobenzene and 30 mL of tetrahydrofuran to a three-necked flask equipped with a stirrer, a thermometer, a gas pipe and a constant pressure dropping funnel, and pass into argon protection. The temperature is -78°C, and the stirring rate is 200r Stir under the condition of / min ...
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Abstract
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