System for spraying catalyst on winding type heat exchange tube bundle

A technology of heat exchange tube bundles and catalysts, which is applied in the field of spraying systems, can solve the problems of complex loading and unloading of catalyst particles, increase the number of heat exchange tube bundles, and uneven distribution of reaction heat, so as to improve the charging efficiency and quality, ensure spraying efficiency, The effect of reducing the charging time

Active Publication Date: 2022-08-02
DALIAN UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, the loading and unloading of catalyst particles is more complicated, and because the position of catalyst particles is fixed and distributed in a bed, the heat of reaction is easily distributed unevenly, resulting in local overheating.
When the heat of chemical reaction is large, the heat dissipation solution is mainly to increase the number of heat exchange tube bundles and increase the heat exchange tube path, and the increase in heat dissipation flux is limited

Method used

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  • System for spraying catalyst on winding type heat exchange tube bundle
  • System for spraying catalyst on winding type heat exchange tube bundle
  • System for spraying catalyst on winding type heat exchange tube bundle

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0056] The following is the preparation of Cu / CeO on the outside of the winding heat exchange tube bundle for the hydrogen production reaction of methanol steam reforming 2 / Al 2 O 3 Examples of thin film catalysts:

[0057] First, CeO is sprayed through the system 2 / Al 2 O 3 vector. Start the electric heating heat medium furnace, heat the heat medium to a predetermined temperature of 80°C, open the third valve 12, start the heat medium circulation pump to send the heat medium to the winding heat exchange tube bundle, and then start the motor to make the tube bundle rotate speed At 15° / s, open the first valve 2a, start the catalyst delivery pump 2, and mix the configured γ-AlOOH solution with CeO with a particle size of 50nm. 2 The powder-mixed catalyst liquid (solid content of 10 wt %) is uniformly sprayed on the surface of the tube bundle from a suitable height. The flow rate of the nozzle is about 2L / min, and the diameter of the formed droplet is about 100μm. The spr...

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Abstract

The invention discloses a system for spraying a catalyst on a winding type heat exchange tube bundle, and relates to the field of chemical engineering and industrial catalysis. The system for spraying the catalyst on the winding type heat exchange tube bundle comprises a catalyst transporting and spraying unit, a heating medium transporting unit, a driving unit and a winding tube prefabricating unit. According to the system, catalyst feed liquid is conveyed, sprayed and recycled to the rotating winding type heat exchange tube bundle through the catalyst conveying and spraying unit, and in the rotating state of the driving unit, a heating medium reaching the preset temperature is introduced into the driving unit through the heating medium conveying unit, so that the catalyst is dried and roasted. According to the system, the mode that a traditional heat exchange type fixed bed reactor is filled with catalyst particles is innovated, the catalyst is sprayed on the winding type heat exchange tube bundle, overall heat exchange catalyst preparation is achieved, catalyst filling and unloading are more convenient, and large-flux heat exchange is achieved; spraying, drying and roasting are synchronously carried out under the continuous rotation of the winding type heat exchange tube bundle, so that the spraying efficiency and the spraying quality are ensured; the system is suitable for preparation of various catalyst systems.

Description

technical field [0001] The invention relates to the fields of chemical engineering and industrial catalysis, in particular to a spraying system for spraying a catalyst on a coiled heat exchange tube bundle. Background technique [0002] The heat exchange fixed bed reactor is a kind of commonly used reactor in the chemical production process. At the same time, the heat exchange between the catalyst bed and the outside is realized. [0003] The catalyst particles and their filling conditions in the reactor have a great influence on the catalytic reaction, and the particle size, bulk density, and adhesion of the active material of the catalyst particles directly affect the reaction rate. However, the loading and unloading of catalyst particles is relatively complicated, and because the catalyst particles are in a fixed position and are distributed in a bed, the reaction heat is easily unevenly distributed, resulting in local flying temperatures. When the chemical reaction hea...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B05B13/02B05B14/00B05B16/20B05D3/02B01J8/02B01J8/06
CPCB05B13/0228B05B13/0278B05B14/00B05B16/20B05D3/0254B01J8/02B01J8/06Y02P20/10
Inventor 代玉强徐琴琴牛硕磊
Owner DALIAN UNIV OF TECH
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