Process for preparing Large ratio surface bata-type aluminium hydroxide
A technology of aluminum hydroxide and large specific surface is applied in the field of preparation of aluminum hydroxide, which can solve the problem that the specific surface of the product is not ideal, and achieve the effect of easy implementation and high purity
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Embodiment 1
[0016] The preparation method of the large specific surface β-type aluminum hydroxide described in the present invention uses the sodium aluminate refined solution obtained by the soda lime sintering method as a raw material, and its composition is that the alumina content is 100g / l, and αk1.44 is diluted with distilled water to The alumina content is 65g / l, and at 34°C, carbon dioxide gas with a concentration of 36% is passed in, and the gas flow rate is 30m 3 / hour·m 3 Solution, after 25 minutes of neutralization reaction, stop feeding carbon dioxide gas, and continue feeding carbon dioxide gas for 65 minutes after 20 minutes, the decomposition rate is 88%. Separate the liquid from the solid, wash and dry the solid to obtain β-type aluminum hydroxide, the content of the product β-type aluminum hydroxide is 90.5%, and the specific surface is 310m 2 / g, and its chemical composition is shown in Table 1.
Embodiment 2
[0018] The preparation method of the large specific surface β-type aluminum hydroxide described in the present invention uses the sodium aluminate refined solution obtained by the soda lime sintering method as a raw material, and its composition is that the alumina content is 100g / l, and αk1.44 is diluted with distilled water to The alumina content is 61g / l, and at 30°C, carbon dioxide gas with a concentration of 36% is passed in, and the gas flow rate is 35m 3 / hour·m 3 Solution, after 20 minutes of neutralization reaction, stop feeding carbon dioxide gas, and continue feeding carbon dioxide gas for 60 minutes after 20 minutes, the decomposition rate is 84%. Separating the liquid from the solid, washing and drying the solid to obtain β-type aluminum hydroxide, the content of the product β-type aluminum hydroxide is 92.4%, and the specific surface is 330m 2 / g, and its chemical composition is shown in Table 1.
Embodiment 3
[0020] The preparation method of the large specific surface β-type aluminum hydroxide described in the present invention uses the sodium aluminate refined solution obtained by the soda lime sintering method as a raw material, and its composition is that the alumina content is 100g / l, and αk1.44 is diluted with distilled water to The alumina content is 56g / l, and at 25°C, carbon dioxide gas with a concentration of 40% is passed in, and the gas flow rate is 40m 3 / hour·m 3 Solution, after 20 minutes of neutralization reaction, stop feeding carbon dioxide gas, continue feeding carbon dioxide gas after 20 minutes for 55 minutes, the decomposition rate is 80%. Separate the liquid from the solid, wash and dry the solid to obtain β-type aluminum hydroxide. The content of the product β-type aluminum hydroxide is 93.2%, and the specific surface is 382m 2 / g, and its chemical composition is shown in Table 1.
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Abstract
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