Preparing process for neohesperidin and use in quality controlling process

A preparation process, a technology of neohesperidin, which is applied in the preparation of sugar derivatives, sugar derivatives, sugar derivatives, etc., can solve problems such as being unable to be used as quantitative detection, hindering market development and going global, and achieves low cost and high improvement. Product quality, cost reduction effect

Inactive Publication Date: 2004-12-08
JIANGXI UNIVERSITY OF TRADITIONAL CHINESE MEDICINE
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AI Technical Summary

Problems solved by technology

Can not meet the needs as a standard product, can only be used qualitatively as a general component, and cannot be

Method used

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Examples

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Embodiment Construction

[0017] Utilize 20-95% ethanol to obtain the extract from the coarse powder of Fructus Fructus Fructus by percolation method; the extract is concentrated and put on a macroporous resin column, and eluted with 20-95% ethanol; the eluate is concentrated and put on Silica gel column, eluted with a mixture of chloroform and methanol, concentrated and left to precipitate crude crystals. The crude crystals are repeatedly recrystallized from methanol to obtain white crystals which are neohesperidin.

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Abstract

A neohesperidine is prepared from such vegetable Chinese-medicinal materials as bitter orange, ash bark, tangerine peel, evodia fruit, etc through extracting in alcohol, adsorbing by macroreticular resin column, separating with silica gel column, eluting, concentrating, and repeated recrystallizing. It can be used in quality control.

Description

technical field [0001] The invention relates to the technical fields of production of pharmaceutical standard products and production and processing of medicinal materials and pharmaceuticals. In particular, it involves the preparation process of the active ingredient neohesperidin and the application of neohesperidin in the fields of medicinal material production, distribution, and quality control of Chinese patent medicines. Background technique [0002] Fructus aurantium, Citrus aurantium, green peel, pomelo peel, tangerine peel, bergamot, and Evodia rutaecarpa are very commonly used varieties in Chinese medicine decoction pieces. varieties. Its main flavonoids are represented by naringin and neohesperidin. Modern pharmacology has proved that it has positive and reliable therapeutic effects in treating gastric and duodenal ulcers, rescuing shock, rescuing heart failure, and treating organ sagging diseases. As traditional Chinese medicine goes to t...

Claims

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Application Information

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IPC IPC(8): C07H1/08C07H17/07
Inventor 付小梅褚小兰范崔生杨武亮
Owner JIANGXI UNIVERSITY OF TRADITIONAL CHINESE MEDICINE
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