Synthetic method for anode material of lithium ion cell
A technology for lithium ion batteries and positive electrode materials, which is applied in battery electrodes, electrode manufacturing, lithium compounds, etc., can solve the problems of environmental pollution, environmental pollution, waste of water resources, etc., and achieves water saving, cost reduction, and elimination of washing steps. Effect
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Embodiment 1
[0012] Embodiment 1: first dissolve cobalt nitrate and lithium hydroxide in water respectively at room temperature, and uniformly mix and react with lithium hydroxide solution and ammonia solution and cobalt nitrate solution, the add-on guarantees Li: Co=1: 1, and the ammonia add-on is Ensure that cobalt ions exist in the form of hydroxide; until the complete reaction does not continue to generate cobalt hydroxide precipitate; dry the cobalt hydroxide precipitate and lithium nitrate solution generated by the reaction at a constant temperature of 200 °C to remove moisture, and keep it at a constant temperature of 900 °C. After firing for 3 hours, lithium cobalt oxide was synthesized.
[0013] The molecular formula of lithium cobaltate is: LiCoO 2
Embodiment 2
[0014] Example 2: At 50°C, first dissolve the mixture of cobalt nitrate, manganese nitrate and nickel nitrate (where Co:Mn:Ni=1:1:1) and lithium hydroxide in water, respectively, dissolve the lithium hydroxide solution and The ammonia solution and the mixture solution are uniformly mixed and reacted, and the addition amount ensures that Li:M=1.02:1 (M represents cobalt, nickel and manganese mixed metal ions), and the addition amount of ammonia water is to ensure that cobalt ions, nickel ions, and manganese ions exist in the form of hydroxides , until the complete reaction does not continue to generate hydroxide precipitation, the hydroxide precipitation and the aqueous solution of lithium nitrate generated by the reaction are removed by spray drying to remove moisture, and calcined at a constant temperature of 900 ° C for 5 hours to synthesize manganese cobalt lithium nickelate .
[0015] The molecular formula of manganese cobalt lithium nickelate is: Li 1.02 Co 0.33 Mn 0.3...
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