Method of manufacturing electroplating cubic boron nitride tool by using surface activation treatment technology
A technology for surface activation treatment and boron nitride tools, applied in the field of preparation of cubic boron nitride tools, can solve the problems of reducing the service life of CBN tools, losing waste, sticking together, and forming blocks, etc., to improve processing efficiency and service life, the effect of enhancing the bonding force
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Embodiment 1
[0042] (1) CBN pretreatment process
[0043] a) Magnetic separation treatment: use a magnet to remove CBN particles with high magnetic induction, and the particle size range of CBN particles is 40 / 45~230 / 270.
[0044] b) Purification and roughening treatment: Soak 20g of CBN particles in 300mL of 10% HCl solution, boil for 30min under constant stirring, rinse with distilled water until neutral after cooling.
[0045] c) Sensitization treatment: the SnCl of 6g 2 2H 2 O was dissolved in 20mL of hydrochloric acid with a concentration of 1.19g / L, and after it was completely dissolved, it was diluted to 500mL with distilled water, and 0.5g of tin particles were added to the sensitization solution for later use. At 25°C, the purified and roughened CBN was immersed in 100 mL of sensitization solution and stirred for 2 min, and then the sensitized CBN particles were washed with distilled water.
[0046] d) Activation treatment: 0.1g PdCl 2Dissolve in 1-2mL hydrochloric acid with a...
Embodiment 2
[0069] Basically the same as Example 1, the difference is
[0070] Is the use of groups into
[0071] SnCl 2 2H 2 O 20g / L
[0072] The concentration is 1.19g / L HCl 40mL / L
[0073] Tin particles 0.3g / L
[0074] CBN soaked in the sensitizing solution at 20°C and stirred for 5 minutes, washed the sensitized CBN particles with distilled water, and then, at 20°C, soaked the CBN in the composition of
[0075] PdCl 2 0.2g / L
[0076] The concentration is 1.19g / L HCl 4- / L
[0077] In the activation solution, stir for 0.5 minutes, wash the activated CBN particles with distilled water, and obtain CBN particles with dispersed palladium particles deposited on the surface
[0078] Finally, soak the CBN in the electroplating solution for sand electroplating.
Embodiment 3
[0080] Basically the same as Example 1, the difference is
[0081] SnCl 2 2H 2 O 40g / L
[0082] The concentration is 1.19g / L HCl 60mL / L
[0083] Tin particles 1.0g / L
[0084] CBN soaked in the sensitizing solution at 30°C and stirred for 10 minutes, washed the sensitized CBN particles with distilled water, and then, at 30°C, soaked the CBN in the composition of
[0085] PdCl 2 0.5g / L
[0086] The concentration is 1.19g / L HCl 10mL / L
[0087] The activated solution was stirred for 1 minute, and the activated CBN particles were washed with distilled water to obtain CBN with dispersed palladium particles deposited on the surface.
[0088] Finally, soak the CBN in the electroplating solution for sand electroplating.
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