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External nickelous sulfate plating liquid circulating purifying device

A cyclic purification, external technology, applied in nickel sulfate and other directions, can solve problems such as large processing, negative impact of plating solution, and inability to continuously electroplating

Inactive Publication Date: 2006-10-25
陈启松
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, the removal efficiency is low, the electrolysis cycle is long, and continuous electroplating is not possible. Electroplating plants generally use the method of working during the day and electrolyzing at night, and scrap products often occur. The plating solution needs to be treated once every half a year on average; , chromium, lead, etc. have good adsorption performance but poor adsorption performance on nickel, which can effectively remove copper, chromium, lead, organic matter and other impurities in the plating solution
However, since activated carbon will adsorb additives (brighteners, wetting agents, etc.) at the same time, it must be replenished after filtration, otherwise it will affect the brightness of the plated parts and increase the stress of the coating, and the carbon fiber is easy to fall off, which will also cause certain damage to the plating solution. Negative impact

Method used

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  • External nickelous sulfate plating liquid circulating purifying device

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Embodiment Construction

[0009] In the accompanying drawings, the plating solution to be purified first enters the pre-reaction zone 3, and after adding the complex impurity removal agent 2, it is circulated and mixed through the water pump 1, so that the medicament and the impurity ions in the plating solution are fully contacted and reacted (medicine Does not react with the main salt), mixed evenly, pumped into the high-level water distribution area 8 through the water pump 1, and flowed into the static diversion sedimentation area 4 by gravity, and the inflow flow can be controlled by adjusting the opening of the electric valve. Under the condition close to static precipitation, it can effectively precipitate and remove impurities in water. After the sediment is dried, copper sulfate can be further recovered. The effluent enters the buffer zone 5, and after being pressurized by the booster pump 6, it enters the microfilter 7, which can remove more than 0.3 μm. The particulate matter and the aging co...

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Abstract

The invention is an external nickel sulfate plating solution circulating purifier, comprising pre-reaction region, static flow guide settling region, buffer region, microfilter, etc, able to effectively remove ions of Cu, Fe, Zn, Pb, Cr, and other impurity metallic ions and aged colloids from the plating solution, and simultaneously not losing main nickel sulfate and additive, and after purified, the impurity content is less than 0.01%. And it adopts external circulating purification process, therefore able to implement continuous production and high-quality plating and able to be widely applied to plating solution purification, nickel sulfate production and purification, etc, in plating industry.

Description

Technical field [0001] The invention relates to an external nickel sulfate plating liquid circulation and purification device, which belongs to the chemical environmental protection category, in particular to a technology capable of effectively removing impurities in the nickel sulfate plating liquid and making them recyclable. Background technique [0002] The traditional electroplating process is generally Cu / Ni / Cr. Before nickel plating, a layer of copper is plated as the bottom layer to improve the bonding force between the surface coating and the metal substrate. Plating parts will inevitably bring some copper ions into the nickel plating process. At the same time, there will be iron, zinc, lead and other impurities introduced in water or additives. When accumulated to a certain extent, the plating layer will appear pinholes, blackening, etc. Affect the quality of plating. With the different levels of electroplating technology, the speed of accumulation is also slightl...

Claims

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Application Information

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IPC IPC(8): C01G53/10
Inventor 陈启松
Owner 陈启松