Root canal appliance prepared from Ti, Mo, Zn, Sn and production method
A production method and root canal technology, applied in the field of TiMoZrSn alloy root canal instruments, can solve problems such as small elastic modulus of NiTi alloy, insensitivity of doctors' hand feeling, and sensitization of patients, etc., achieve small elastic modulus, eliminate toxicity and Allergic reaction, high efficiency of residual marrow
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Embodiment 1
[0044] Example 1: 1100g of pure molybdenum powder, 500g of pure zirconium wire, 400g of pure tin wire, and 8000g of titanium sponge.
Embodiment 2
[0045] Example 2: 1000g of pure molybdenum powder, 450g of pure zirconium wire, 525g of pure tin wire, and 8025g of titanium sponge.
Embodiment 3
[0046] Example 3: 1300g of pure molybdenum powder, 750g of pure zirconium wire, 375g of pure tin wire, and 7575g of titanium sponge.
[0047] 1. Smelting of materials
[0048] Using the vacuum consumable electrode arc melting method, the raw materials of pure molybdenum powder, pure zirconium wire, pure tin wire and sponge titanium are pressed into consumable electrodes. The melting voltage ranges from 20V to 50V, the current ranges from 1000A to 3000A, and the vacuum degree is not lower than 10 -2 Pa, to obtain the ingot billet, such as Figure 11 shown.
[0049] 2. Processing of billets
[0050] Remove the riser from the ingot, peel off the surface on a lathe to remove defects such as scale and subcutaneous pores, and polish the billet to remove defects such as folds, heavy skin, cracks, etc., and then hold it at 950°C for 2 hours to forge it into a 70mm×70mm square billet , and then gradually forged into a 30mm×30mm square billet, and then rolled into a circle. Rotate ...
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