Preparation method of cassava hydroxypropyl distarch glyceride
A technology for tapioca hydroxypropyl distarch glycerol and tapioca starch, which is applied in the field of preparation of tapioca hydroxypropyl distarch glycerol ether, can solve the problems of unevenness, poor product quality, small seeds in planting area, etc., and achieves low production cost , high-quality, high-transparency effects
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[0022] Embodiment 1: at first 100 kilograms of tapioca starch, 15 kilograms of sodium sulfate and 180 kilograms of water are adjusted into 20-23Be starch slurries in the reactor, constantly stirring, adding mass concentration in the still is 3-4.0% sodium hydroxide solution to regulate The pH value was 11.0, alkalized for 40 minutes, added 4.5 kg of propylene oxide, kept the temperature at 42 ° C and made it react, reacted for 10 hours and added 5ml of epichlorohydrin, continued to react for 25 hours, and added a mass concentration of 8-10% hydrochloric acid solution Neutralize to pH 6.0-7.0, add 200 kilograms of water to the kettle to wash, settle, and then wash in the same way to remove impurities (sodium sulfate, sodium chloride or other chemical residues) to obtain the finished product.
Example Embodiment
[0023] Example 2: The steps are the same as those in Example 1, except that the amount of propylene oxide added in the etherification process is 4.0 kg, and the reaction temperature is maintained at 40°C.
Example Embodiment
[0024] Example 3: The steps are the same as those in Example 1, except that the amount of propylene oxide added in the etherification process is 4.0 kg, and the reaction temperature is maintained at 45°C.
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