Cubic boron nitride sintered compact
A technology of cubic crystal and sintered body, which is applied in the field of cubic boron nitride sintered body, which can solve problems such as defective cBN particles, wear, and difficulty in reaction, and achieves suppression of defect or wear, high thermal conductivity, and excellent damage resistance. Effect
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Embodiment 1
[0031] cBN powder and binder powder having an average particle diameter of 2 μm were prepared. This binder powder was produced by mixing 50% by weight of Co, 40% by weight of Al, and 10% by weight of WC. The bonding material powder and the cBN powder with an average particle diameter of 2 μm were mixed using a cemented carbide pot and balls. This powder was filled in a cemented carbide container, and sintered at a pressure of 6.0 GPa and a temperature of 1400° C. for 30 minutes.
[0032] Table 1 shows cBN sintered bodies produced by changing the type of cBN powder and the ratio of cBN powder to binder powder. The content of cBN and the amount of catalyst elements were measured by the following methods. First, in order to measure the amount of elements contained in the cBN sintered body, the sintered body was melted by the molten salt method, and then each element was quantitatively measured by high-frequency induction plasma emission analysis (ICP method). From the results,...
Embodiment 2
[0050] Using the sintered body material produced in Example 1, thermal cracking and thermal conductivity were evaluated. Thermal conductivity was obtained using the laser flash method or AC calorimetry. In addition, a cBN sintered body was added to obtain a cutting insert in the shape of ISO standard SNGA090312. Using these cutting inserts, cutting evaluation was performed under the following conditions, and the number of thermal cracks was evaluated.
[0051] Cutting material: gray cast iron FC250 milling
[0052] Cutting conditions: cutting speed V=2500m / min, cutting depth Rd=30mm, Ad=0.3mm
[0053] Feed rate f=0.2mm / knife, dry type, cutting time 30 minutes
[0054] Table 2 shows the obtained results.
[0055] According to the comparison of samples 1 to 6, it was found that sample 1 with a cBN content of less than 70% by volume had defects that were considered to be caused by thermal cracks, and the number of thermal cracks could not be evaluated, while samples 2 to 6 pr...
Embodiment 3
[0061] Using the sintered body material produced in Example 1, chipping resistance was evaluated. First, cutting inserts in the shape of ISO standard SNGA120408 were produced. Using these cutting inserts, cutting evaluation was performed under the following conditions, and the time to chipping was evaluated.
[0062] Cutting material: gray cast iron FC300 round bar outer diameter turning with 6 V-shaped grooves
[0063] Cutting conditions: cutting speed V=700m / min, cutting depth d=0.5mm
[0064] Feed f=0.2mm / rev., dry type
[0065] Table 2 shows the obtained results.
[0066] According to the comparison of samples 1 to 6, it was found that sample 1 with a cBN content of less than 70% by volume produced defects at the initial stage of cutting, reaching 1 / 6 to 1 / 8 of the defect life of samples 2 to 5 produced based on the scope of the present invention. This is because the cBN content of sample 1 outside the scope of the present invention was small, and a skeleton structure ...
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