Method of making ultrafine crystal deformed aluminium alloy
A technology of deforming aluminum alloy and ultra-fine grain, which is applied in the field of materials, can solve the problems of unsatisfactory effect and high cost of pulse current, and achieve the effect of refining grain, improving mechanical properties and increasing supercooling degree
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Embodiment 1
[0016] In the experiment, 6351 aluminum alloy was prepared with industrial pure Al and industrial pure Mg, Al-Si, Al-Mn master alloy. The alloy composition was 0.7-1.3% Si, 0.4-0.8% Mn, 0.4-0.8% Mg, and the balance was Al. First put pure aluminum into a crucible to melt and heat up to 800°C, and cover it with JZF-03 high-temperature covering agent; add alloy elements, add JZJ type harmless aluminum alloy refining agent for degassing and refining, remove scum, and then After standing at 730°C for 20 minutes, pour it into a water-cooled copper mold (Φ80mm×200mm), the water flow rate is 2.2ml / s, mechanical vibration is carried out during the solidification process, the vibration frequency is 50Hz, the excitation force is 100N, and 6351 is obtained after solidification Ingot. The alloy homogenization treatment process is: 463℃×24h to eliminate composition segregation. The hot extrusion process is as follows: the preheating temperature is 450° C., the extrusion speed is 1 m / min, a...
Embodiment 2
[0018] In the experiment, 2024 aluminum alloy was prepared with industrial pure Al and Al-Cu, Al-Si, Al-Mn master alloy. The alloy composition was 3.8-4.9% Cu, 0.3-0.9% Mn, 1.2-1.8% Mg, and the balance was Al. First put pure aluminum into a crucible to melt and heat up to 800°C, and cover it with JZF-03 high-temperature covering agent; add alloy elements, add JZJ type harmless aluminum alloy refining agent for degassing and refining, remove scum, and then After standing at 750°C for 20 minutes, pour it into a water-cooled copper mold (Φ80mm×200mm), the water flow rate is 2.2ml / s, mechanical vibration is performed during the solidification process, the vibration frequency is 45Hz, and the excitation force is 90N. After solidification, 2024 Ingot. The alloy homogenization treatment process is: 463℃×24h to eliminate composition segregation. The hot extrusion process is as follows: the preheating temperature is 450° C., the extrusion speed is 1 m / min, and the extrusion ratio is 3...
Embodiment 3
[0020] In the experiment, 7075 aluminum alloy was prepared with industrial pure Al and industrial pure Mg, Al-Cu, Al-Zn, Al-Cr master alloy. ~6.1% Zn, the balance is Al. First put pure aluminum into a crucible to melt and heat up to 800°C, and cover it with JZF-03 high-temperature covering agent; add alloy elements, add JZJ type harmless aluminum alloy refining agent for degassing and refining, remove scum, and then After standing at 750°C for 20 minutes, pour it into a water-cooled copper mold (Φ80mm×200mm), the water flow rate is 2.2ml / s, mechanical vibration is carried out during the solidification process, the vibration frequency is 40Hz, and the excitation force is 80N. Get 7075 ingot after solidification. The alloy homogenization treatment process is: 463℃×24h to eliminate composition segregation. The hot extrusion process is as follows: the preheating temperature is 450° C., the extrusion speed is 1 m / min, and the extrusion ratio is 30:1. The heat treatment process o...
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