53 results about "Cunife" patented technology

The invention relates to a high-thermal-conductivity graphite-aluminium composite material reinforced by diamond particles in a hybrid manner and a preparation process for the same. The composite material is composed of, in volume fraction, 21-41% of diamond, 32-65% of flake graphite, and the balance of aluminium or aluminium alloy. The preparation process comprises the following steps of: (1) uniformly mixing diamond particles and flake graphite to obtain mixed powder; (2) adding a polyvinyl alcohol (PVA) solution in the mixed powder and stirring, and pressing to obtain a precast block; (3) preheating and gluing the precast block in a die; (4) heating and melting aluminium or aluminium alloy in a crucible to 700-900 DEG C, then pouring an aluminium melt or aluminium alloy melt in the die; (5) applying an axial pressure by a hydraulic machine, and enabling the aluminium melt or aluminium alloy melt to infiltrate in pores in the precast block; and (6) cooling and releasing the die, and taking out the composite material. Compared with the prior art, the composite material obtained by the preparation process disclosed by the invention has a high thermal conductivity and obtains a high mechanical property simultaneously.

The invention relates to a preparation method of RE-Mg-Ni-M based hydrogen storage alloy. Under the protection of inert gases, the as-cast condition products of the RE-Mg-Ni-M based hydrogen storage alloy are smelted through using a cold-crucible magnetic-suspension furnace; heat-treated products are obtained by heat treatment of the as-cast condition products. The method has the steps that: (1) material is prepared; (2) metal Ni and M are smelted together; (3) metal RE is smelted; (4) the casting ingots obtained from step (2) and step (3) are smelted; (5) the ingot obtained from step (4) is overturned and smelted to obtain alloy solution, then master alloy of magnesium is added into the alloy solution to obtain the as-cast condition products of the RE-Mg-Ni-M based hydrogen storage alloy by cooling; (6) heat treatment is carried out to the as-cast condition products to get the heat-treated product. The single weight of the as-cast condition products and heat-treated products is 50-1000g; the content of magnesium in the products is close to designed content; the components of the as-cast condition products are uniform and have high hydrogen storage capacity; the structure and components of the heat-treated products are uniform and also have high hydrogen storage capacity and long cycling life.

The present apparatus is comprised by two magnetic induction sets, one for melting of the raw material and the second for purification of molten metal; each set comprises a pot or crucible (1, 1'), an electromagnetic device, a filter (11) and a power supply; each crucible (1, 1') is surrounded in the lower part by a hollow permanent magnet (3, 3') in which three pairs of electromagnets facing each other are arranged; the process consists of the following stages: a) charging of metallic raw material inside a crucible (1); b) electromagnetic induction heating to melt the metallic raw material (2) inside crucible (1) through a three-phase magnetic system creating a horizontal travelling or pules magnetic field which builds a turbulent flux inside the melt (2'); c) whirling stirring of melt (2') by electromagnetic induction and purification of it via extraction of hydrogen and of non-electroconductive inclusions by coagulation of them in agglomerates; d) discharging of purified melt (2') by a magneto-hydrodynamic pump effect for the next treatment or technological actions such as the continuous or periodical casting through a filter for the mechanical filtration of the agglomerates.

The invention provides silver-copper-tin alloy, a silver-copper-tin alloy brazing wire prepared by using the silver-copper-tin alloy and a preparation method for the silver-copper-tin alloy brazing wire. The silver-copper-tin alloy consists of the following ingredients in percent by weight: 25-35wt% of copper, 5-18wt% of tin and the balance silver. The silver-copper-tin alloy brazing wire is excellent in welding performance, and is an important intermediate-temperature brazing wire for an electric vacuum device; and the problem that an electronic device is failed due to over high brazing temperature is effectively solved. The preparation method comprises the following steps of selecting high-purity silver, oxygen-free copper and high-purity tin; calculating the required quantities of the high-purity silver, the oxygen-free copper and the high-purity tin according to a matching range; preparing materials; placing matched furnace materials in a crucible of a double-vacuum continuous casting machine; refining the furnace materials after the furnace materials are totally melted; regulating the temperature to 730-760 DEG C; beginning to perform casting at the speed of 1.5mm/s after standing for a moment; stopping 2 seconds after performing casting for 1 second; performing multi-pass rotary swaging and online annealing on cast ingots; enabling the diameters of the cast ingots to be reduced to 3.4 mm from 8mm by rotary swaging; and performing wiredrawing, vacuum annealing, peeling treatment and cleaning so as to obtain a threadlike finished product with the diameter of 0.5mm. The preparation method is simple; and the problem that the silver-copper-tin alloy is quite easy to oxidize in a machining and forming process is solved.

The invention provides low-cost high-strength alpha+beta titanium alloy. The titanium alloy takes titanium as a main body element, and takes alpha stable elements, namely, Al and B, and beta stable element, namely, Fe, as alloy elements; and the titanium alloy is prepared from the following components in percentage by weight: 2.5 to 4.5 percent of Al, 2.5 to 4 percent of Fe, 0.05 to 0.2 percent ofB, and the balance of titanium and unavoidable impurities. The invention also provides a preparation method of the low-cost high-strength alpha+beta titanium alloy; the preparation method comprises the following steps: adding raw materials into a water-cooled crucible suspension melting furnace into which argon gas is introduced according to a designed proportion alloy component proportion; obtaining an ingot casting after repeated melting; cogging and forging above a phase transition point; sampling a forged alloy and performing heat treatment; and finally, characterizing tissue structures and performance. The prepared titanium alloy is uniform in alloy components and fine in tissues; the tensile strength is greater than or equal to 1,000 MPa, and the plastic elongation percentage is greater than or equal to 15 percent; and the alloy has the advantages of low cost and high strength, and can replace part expensive titanium alloys in certain fields.

Provided are a liquid phase growth method including a step of immersing a substrate in a crucible storing a solvent having a growth material dissolved therein; and a step of cooling the solvent from an interior thereof, and a liquid phase growth apparatus for use in the method, by which a temperature difference of a solution is decreased and by which a deposited film is formed in a uniform thickness.

The invention provides a silver-magnesium-nickel friction ring manufacturing method. The method includes the following steps: cleaning the furnace wall of a vacuum intermediate-frequency sensing furnace and raw materials; subjecting the raw materials to smashing and degassing; smelting under the condition of 5-10Pa in vacuum degree to obtain silver-nickel intermediate alloy; using a silver piece to coat magnesium, using a silver wire to bind the silver-nickel intermediate alloy at the upper end of a crucible, and smelting to obtain silver-magnesium-nickel alloy ingots; using a dilute sulfuric acid solution to remove an oxidation film on the surface of each ingot, processing the ingots whose ingredients, interiors and surfaces are all qualified, using a hydraulic press to flattening a plate after being rolled and cogged, and performing cold forging or hot forging on a bar for many times to enable the bar to meet hardness requirements; adopting wire-electrode cutting and a milling machine to process the plate and the bar into blank rings respectively, using a turning lathe to process the blank rings to be in the size of finished products, and adopting ultrasonic waves and X-ray lossless detection to perform product interior quality detection. A silver-magnesium-nickel friction ring obtained by the method is smooth and flat in surface and free of defects like cracking, peeling and corrosion discoloring.

The invention relates to biodegradable, metal alloy-containing compositions, methods for their preparation and applications for their use. The compositions include magnesium and other components, such as yttrium, calcium, silver, cerium, and zirconium; or zinc, silver, cerium, and zirconium; or aluminum, zinc, calcium, manganese, silver, yttrium; or strontium, calcium, zinc. The compositions are prepared by vacuum induction/crucible melting together the components and casting the melted mixture in a preheated mild steel/copper mold. In certain embodiments, the compositions of the invention are particularly useful for forming medical devices for implantation into a body of a patient.

In a method for producing a coupling on a pipe, preferably consisting of copper or steel or Cu-, Ni-, Fe-alloys, by way of a preferably graduated or one-stage expansion of the pipe end to create a much larger difference in diameter, an expansion tool is introduced axially into the end of the pipe. Once the expansion tool has been introduced into the pipe end, the region of the pipe end that is to be or has been expanded is completely or partially compressed, by a force acting axially on the pipe end, so that the external diameter of the pipe end that is to be processed is delimited by one or more shaping jaws that completely or partially surround the pipe end. The invention also relates to a device for producing a coupling on a pipe end according to the method.

The invention relates to a hot-dipping technological method and device for preparing a component gradient alloy material. According to the method, the alloy material is directly prepared on the surface of a base material, and the component gradient coating alloy or magnesium alloy is prepared rapidly. The method specifically includes the following steps that (1) a steel (or nickel or copper or other high-melting-point material) wire or band serves as the base material; (2) the alloy is melted in a crucible; (3) after being subjected to surface treatment, the base material penetrates through molten alloy for hot dipping; (4) alloy elements are added to change the components of the molten metal; and (5) the alloy material with the components varying in the motion direction of the base material is obtained. By means of the method, a large number of component gradient alloy coatings within a certain component range can be prepared within a short period, and the prepared finished products can be used as samples for a high-throughput experiment. Compared with other preparation methods for samples of the high-throughput experiment, the method is high in efficiency and low in cost, and the prepared material can be subjected to subsequent machining.

The single crystal extraction method is used for shortening the extraction time from the forming of a straight body part to crystal excision from a meltwater, extracting single crystal and improving a rate of finished products. The method comprises a first process, a second process and a third process. The first process forms the straight body part (C2), and the second process is behind the first process. In the final process of forming the straight body part, a lower protruded shape (C3) protruded downwards is formed at the lower end of the crystal, and the third process is configured to cut the lower protruded shape formed in the second process from the silicon meltwater. In the second process, the field density of the horizontal magnetic field is controlled lower than the first process in the range of 800 to 1000 gausses, the crystal extract speed is controlled lower than the first process in the range of 0.2 to 0.5 mm/min, the crystal rotation speed is controlled lower than the first process in the range of 1 to 3 rpm, and the crucible rotation speed is controlled in the range of 0.5 to 5 rpm.

The invention relates to a preparation method of titanium or titanium alloy powder with micro-hydrogenated surface. The method comprises the following steps: (1) a titanium or titanium alloy bar with low pollution and specific size is prepared in advance; (2) an atomizing unit is pre-vacuumized and then filled with high-purity inert gas as shielding gas; (3) the lower end of the titanium or titanium alloy bar is heated to be melted by an induction coil, and atomized power preparation is performed; (4) titanium or titanium alloy powder obtained after atomization enters a cyclone separator, hydrogen is introduced into the cyclone separator, and low-temperature surface micro-hydrogenation treatment is finished in the cyclone separator; (5) after the powder is cooled completely, the titanium or titanium alloy powder with micro-hydrogenated surface is taken from a powder collecting tank. Aiming at the problem of high probability of oxidation of titanium or titanium alloy powder surface, crucible-free atomization and low-temperature surface micro-hydrogenation are combined, and the titanium or titanium alloy powder with the micro-hydrogenated surface, little pollution and excellent oxidation resistance for 3D printing is prepared.

The invention discloses a preparation method of a hypereutectic aluminum-silicon alloy casting. The preparation method comprises the following steps of: (1) preheating a crucible, putting AlSi alloy, AlCu alloy and AlNi alloy into the crucible, heating the alloys, and pressing metallic magnesium into the molten materials; (2) pressing inoculant into the alloy melt, stirring the melt uniformly, and then preserving the heat; (3) pressing ZnCl2 into the alloy melt, removing slag after heat preservation and degassing, and casting the melt into a casting blank; and (4) performing heat treatment on the casting blank, and thus obtaining the hypereutectic aluminum-silicon alloy casting. The mechanical property of the product prepared by the method is superior to that of a similar hypereutectic aluminum alloy product; and the method is simple, easy to realize industrialization and low in preparation cost.

The invention relates to heatproof magnesium stannum silver alloy and a preparation method thereof, which belongs to metal structural materials and the field of preparation technology. The ingredient of the magnesium stannum silver alloy is composed of four elements of magnesium, stannum, silver and manganese or five elements of magnesium, stannum, silver, manganese and zinc. The mass percentage of the content of each ingredient is stannum (Sn) of 6% to 7%, silver (Ag) of 1% to 2%, manganese (Mn) of 0.2 % to 0.5%, zinc (Zn) of 0% to 1.0% and magnesium of the rest. The preparation method comprises steps of sequentially placing all ingredients in a crucible, heating, stirring, standing to form alloy liquid, pouring into cold molds to form blanks of the magnesium stannum silver alloy, heating in the air, quenching in cold water to obtain homogenized magnesium stannum silver alloy and finally performing aging hot treatment in the air and quenching in cold water to achieve the heatproof magnesium stannum silver alloy. The magnesium stannum silver alloy is small in content of elements and simple in smelting technology. Under 200 DEG C, the aging peak value can reach more than 84 HV. Aging of 700 hours, hardness can keep above 77 HV. Thus, high temperature tissues are stable, and commercial potentiality is provided.

The invention discloses a drawing method for a C-shaped silicon core, wherein in the method, a crucible (5) and a heating sleeve (6) used for melting a crystal (7), and a die plate (11) structure for drawing the C-shaped silicon core (2) are provided. The drawing method comprises the following steps of: A, previous preparation, B, melting for the materials of the crystal (7), C, control for the silicon core, and D, finishing for the C-shaped silicon core (2), wherein many times of drawing for the C-shaped silicon core (2) of a crystal drawing process can be realized by repeating the steps aforementioned. During the subsequent use of the drawing method disclosed by the invention, the disadvantage of small diameter of the existing solid square silicon core or circular silicon core is effectively overcome; the purpose of rapidly growing a polycrystalline rod is realized by the C-shaped silicon core having a weight which is equal to or slightly greater than the weight of the solid silicon core; and the method for drawing the silicon core disclosed by the invention is simple to cost, and capable of greatly saving enterprise cost.

The invention provides a multi-alloying beta-phase-solidified high Nb-TiAl alloy and a preparation method thereof, and belongs to the technical field of alloy. The alloy comprises the following elements in molar percentage: 43-45% of Al, 5-15% of Nb, no greater than 0.2% of W, no greater than 0.5% of Cr, and the balance of Ti and inevitable impurities; raw materials are formed by briquetting according to the ratio; firstly, a titanium sponge is placed on the inner edge of a mold; secondly, a high pure aluminium layer, an aluminium niobium middle alloy layer, an electrolyzed chromium piece, an aluminium tungsten niobium middle alloy layer, and a titanium sponge layer are arranged sequentially from the bottom up respectively; the briquetting is placed a water cooled copper crucible vacuum induction suspend smelting furnace capable of realizing centrifugal casting; the melt is obtained through smelting under vacuuming, and is mixed uniformly; the melt is cast into a metal mold which is preheated and perform centrifugal rotation for performing centrifugal rotation,, and is cooled along with the furnace. According to the method, the uniform fine TiAl alloy without obvious segregation is obtained.

The invention belongs to the field of metal materials, aims at the technical problem that high strength and high thermal conductivity cannot be both considered in an existing magnesium alloy, and specifically discloses a high-thermal-conductivity rare-earth magnesium alloy. The magnesium alloy contains 2.5-3.5wt.% of zinc, 0.15-0.35wt.% of zirconium, 0-1.5wt.% of samarium and the balance magnesium and inevitable impurities. The invention further discloses a preparation method for a high-thermal-conductivity rare-earth magnesium alloy. The preparation method comprises the following steps: 1) weighing a pure magnesium ingot, pure zinc particles, an Mg-Zr intermediate alloy and an Mg-Sm intermediate alloy according to the required component contents for standby; 2) drying and preheating the raw materials weighed in the step 1) at 200 DEG C for 2h separately for standby; 3) placing the pure magnesium ingot preheated in the step 2) in a stainless steel crucible, and heating the pure magnesium ingot under the shield of a protective gas; and 4) carrying out hot extrusion deformation on the magnesium ingot in the step 3), thereby obtaining the deformed magnesium alloy.

The invention provides a device for non-vacuum smelting easy- to-oxidize metals and alloys, and its main parts comprise furnace body and furnace cover, where the furnace body is equipped with a heater, and a pot is placed inside the furnace body; and the furnace cover has an gas inlet, an gas outlet and a feed inlet and is equipped with a cooling mechanism; the bottom of the hearth is equipped with a bottom pouring orifice, a vertical stopper is arranged inside the furnace body, the lower end of the stopper is connected with the bottom pouring orifice, the upper end of the stopper is equipped with an adjustment mechanism which adjusts the vertical position of the stopper to prevent metal melt from flowing down in the smelting course; the lower side of the furnace body is directly connected with a crystallizer or iron mold, it adopts a down-pouring mode and the connecting channel is made with an gas inlet and an gas outlet. And its whole smelting and casting course is performed in the industrial pure protective gas, having low melting loss rate and good deoxidizing and dehydrogenating effects, easy to implement large-scale continuous operation and obviously improving the pouring quality.

The invention provides a production method of low-price rapidly quenched magnetic powder containing lanthanum and cerium. The method comprises the following steps of loading raw materials into a crucible according to the order of a first layer of iron, zirconium, ferroboron, a second layer of iron, lanthanum cerium and praseodymium neodymium; starting a smelting furnace for preheating and discharging an adsorbed gas in the raw materials; further increasing power until the raw materials are completely melted, pouring and obtaining a uniform alloy; carrying out rapid quenching treatment on the alloy to obtain an alloy strip; finally carrying out crystallization treatment on the alloy strip, wherein the composition formula of the magnetic powder is (LaCe+PuNd)<x>(FeZr)<84.5-x>B<6.5>, wherein X is 9-11 and the ratio of LaCe:PuNd is 1:(0.2-4). One part of praseodymium neodymium is replaced with the lanthanum cerium, so that the residual magnetic flux density Br of the prepared magnetic powder is (5-7.5)kGs, the intrinsic coercive force Hcj is (6-9.5)kOe and the maximum magnetic energy product BH is (6-12)MGOe. The magnetic powder is suitable for the market requirements, the cost of the raw materials is reduced and a new application way is opened up for highly abundant rare earth.

The invention discloses a method for preparing a copper-chromium composite contact material through an electron beam cladding process. The method comprises the following steps: (1) preparation of a base body material; (2) preparation of cladding powder: mixing copper powder and chromium powder according to a ratio, then adding absolute ethyl alcohol, and carrying out ball grinding on the mixed powder through a copper ball to obtain the cladding powder; (3) spreading: spreading the cladding powder on the surface of an oxygen-free copper block; (4) pressing: pressing the cladding layer with a press, and carrying out natural airing or drying; (5) vacuumizing: putting a pressed sample into electronic beam equipment, and vacuumizing to 10<-2> pa or below; (6) electron beam scanning: melting the cladded copper-chromium powder through electron beam scanning, and enabling the surface of an oxygen-free copper base body to be slightly melted to form metallurgical bonding between the copper-chromium powder and the oxygen-free copper base body. According to the preparation method disclosed by the invention, the raw materials are not in contact with a crucible, so that inclusions caused by falling of the crucible and relatively high product gas content caused by crucible degassing are avoided; and meanwhile, by rapid cooling, the particle size of a product from the edge part to the heart part is uniform and fine.