Gas generant materials
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example 1
[0065] The same procedure as in Comparative Example 1 except that, 1) 5-aminotetrazole and bCN were reacted in water at 190° F. for 1 hour in order to make the 5-AT / bCN complex and 2) cupric oxide and diammonium bitetrazole were reacted in water at 190° F. for 1 hour in order to make the copper diammonium bitetrazole prior to the addition of the other ingredients.
TABLE 1CE 1CE 2CE 3Example 1GN50.3827.4924.6628.58bCN46.6214.3551.7221.36CuDABT——20.624.00bCuATN—55.16—43.36Al2O32.701.501.501.50SiO20.301.501.501.20
where,
[0066] GN=guanidine nitrate
[0067] bCN=basic copper nitrate
[0068] CuDABT=copper diammonium bitetrazole and
[0069] bCuATN=5-amino tetrazole substituted basic copper nitrate
[0070] The gas generant formulation of each of Comparative Examples 1-3 and Example 1 was then tested. The burn rate and combustion flame temperature (Tc) values identified in TABLE 2 below were obtained. In particular, the burn rate data was obtained by first pressing samples of the respective gas...
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