Flame-retardant fiber composite and fabric produced therefrom
a technology of flame-retardant fibers and fibers, which is applied in the field of flame-retardant fiber composites, can solve the problems of insufficient realization of flame-retardant materials, safety of health, and omission of washing, so as to improve the processability and bulkiness, and the effect of satisfactory touch and feeling
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manufacturing example 1
[0082] A copolymer comprising 51% by weight of acrylonitrile, 48% by weight of vinylidene chloride, and 1% by weight of p-sodium styrene sulfonate was dissolved so that a resin concentration might give 30% by weight into dimethylformamide. Antimony trioxide 15 parts was added to 100 parts of a resin weight of the obtained resin solution to obtain a spinning solution.
[0083] The antimony trioxide had a particle diameter uniformly adjusted to not more than 2 micrometers, and was beforehand adjusted so that it might disperse uniformly in a diluting resin solution.
[0084] A spinning solution including antimony trioxide was extruded into an dimethylformamide aqueous solution with a concentration of 50% by weight, using a nozzle having a diameter of nozzle hole of 0.08 mm, and a number of holes of 300 holes. The obtained fiber was dried at 120 degrees C. after washing with water, subsequently, after drawing at 3 times, heat treatment was given at 145 degrees C. for 5 minutes to obtain a f...
manufacturing example 2
[0086] A copolymer comprising 56% by weight of acrylonitrile, 41% by weight of vinylidene chloride, and 3% by weight of sodium 2-acrylamide-2-methylpropanesulfonate was dissolved into dimethylformamide so that a resin concentration might give 20% by weight. Antimony trioxide was added into the obtained resin solution to give a spinning solution. Table 1 shows amounts of addition of antimony trioxide.
[0087] The antimony trioxide had a particle diameter uniformly adjusted to not more than 2 micrometers, and was beforehand adjusted so that it might disperse uniformly in a diluting resin solution.
[0088] A spinning solution including antimony trioxide was extruded into an dimethylformamide aqueous solution with a concentration of 50% by weight using a nozzle having a diameter of nozzle hole of 0.08 mm, and a number of holes of 300 holes. The obtained fiber was dried at 120 degrees C. after washing with water, and subsequently, after drawing at 3 times, heat treatment was given at 145 d...
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