Use of fragrance compositions for the prevention of the development of indole base malodours from fecal and urine based soils
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example 1
Identification of Active Fragrance Compounds
[0067]A sample of fresh human urine is divided into equal portions and a fragrance containing one or more of the effective materials was added as described in the Indole Inhibition Test. Control samples were prepared in which inactive compounds were substituted and a third unfragranced blank was also prepared to determine the suitability of the urine. The samples were stored and after 24 hours the indole content and fragrance active content is measured by gas chromatography with mass spectrometric (GCMS) detection. Those formulations containing active ingredients prevented the formation of indole while both the unfragranced and the alcohol containing control samples had much greater quantities of indole present. Also for the active compounds a GCMS measurement indicated the extent to which the compound was itself consumed as part of the process. In table 2 the decrease in fragrance components has been classified into 3 categories and the l...
example 2
Performance from a Liquid Rim Block
[0069]The active composition of Table 3 (example 2) was mixed into a liquid rimblock formulation having the composition of example 6 of which 0.25 g was added to 7.0 g of a fresh suitable human urine sample to give 0.02 g of active fragrance as described in part B of the indole inhibition test. After 24 hours the indole content was measured and the result shown as file URIN40.D in FIG. 1. Comparative example A control was mixed with the same liquid rim block formulation and gave the results in file URIN41.D in FIG. 1 while a blank sample containing 0.2 g of the liquid rim block formulation in urine gave file URIN39.D in FIG. 1. It can be seen the fragrance composition of the invention reduced indole concentration below 0.01 ppm (wt / wt). Note that the dosage of example 2 and comparative A in the liquid rim block represents about 30% of the normal total fragrance dose.
TABLE 3Effectiveness in a Liquid Rim Block - Formulation ofActive ComponentsExample...
example 3
[0070]Table 4 below demonstrates a fragrance composition according to the present invention containing 5% of active ingredient suitable for use in household products, along with a control fragrance comparative example B containing the corresponding inactive alcohols to the active aldehydes.
TABLE 4Example of Effective and Ineffective FragrancesExample 3Comparative Example BCompound%Compound%Benzaldehyde5Benzyl alcohol5Geraniol 98%20Geraniol 98%20Geranium oil Egypt nat2Geranium oil Egypt nat2Verdox5Verdox5Manzanate5Manzanate5Musk t-935Musk t-935Phenyl acetaldehyde10Phenyl ethyl alcohol10Phenyl ethyl alcohol42Phenyl ethyl alcohol42Phenylethylphenylacetate5Phenylethylphenylacetate5Rose oxide1Rose oxide1
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