Monomeric fc domains
a technology fc domains, applied in the field of monomeric fc domains, can solve the problems of long serum half-life, short half-live of many of these formats compared to full-size iggs, and risk of immunogenicity, and achieve the effect of reducing toxicity
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example 1
Construction of Bispecific Monomeric Tandem CH3 Fc Polypeptides
Materials and Methods
[0174]Different constructs were made for use in the preparation of a bispecific Fc-polypeptide based on a scFv specific for human tumor antigen CD19 (anti-CD19 scFv) and a scFV specific for human activating receptor NKp46 on NK cells (anti-NKp46 scFv).
[0175]Shown below in Table 1 are the light chain and heavy chain variable regions amino acid sequences for the anti-CD19 component of the proteins.
TABLE 1Anti-CD19SequenceAnti-CD19-VK DNASEQ ID NO: 3Anti-CD19-VK amino acidSEQ ID NO: 4Anti-CD19-VH DNASEQ ID NO: 5Anti-CD19-VH amino acidSEQ ID NO: 6
[0176]Shown below in Table 2 are the light chain and heavy chain variable regions and scFv amino acid sequences for the anti-NKp46 component of the proteins.
TABLE 2Anti-NKp46scFV sequence (VHVK) / - stopNKp46-3 VH amino acidSEQ ID NO: 7NKp46-3 VL amino acidSEQ ID NO: 8NKp46-3 scFv amino acidSEQ ID NO: 9
Cloning and Production of the Recombinant Proteins
[0177]Coding...
example 2
NKp46 Binding Affinity by Bispecific Proteins by Surface Plasmon Resonance (SPR)
Biacore T100 General Procedure and Reagents
[0213]SPR measurements were performed on a Biacore T100 apparatus (Biacore GE Healthcare) at 25° C. In all Biacore experiments HBS-EP+ (Biacore GE Healthcare) and NaOH 10 mM served as running buffer and regeneration buffer respectively. Sensorgrams were analyzed with Biacore T100 Evaluation software. Protein-A was purchase from (GE Healthcare). Human NKp46 recombinant proteins were cloned, produced and purified at Innate Pharma.
Immobilization of Protein-A
[0214]Protein-A proteins were immobilized covalently to carboxyl groups in the dextran layer on a Sensor Chip CM5. The chip surface was activated with EDC / NHS (N-ethyl-N′-(3-dimethylaminopropyl) carbodiimidehydrochloride and N-hydroxysuccinimide (Biacore GE Healthcare)). Protein-A was diluted to 10 μg / ml in coupling buffer (10 mM acetate, pH 5.6) and injected until the appropriate immobilization level was reache...
example 3
NKp46 Mechanism of Action
[0219]NKp46×CD19 bispecific proteins having an arrangement according to the F3 format described in Example 1 were compared to rituximab (anti-CD20 ADCC inducing antibody), and a human IgG1 isotype control antibody for functional ability to direct CD16- / NKp46+ NK cell lines to lyse CD19-positive tumor target cells.
[0220]Briefly, the cytolytic activity of the CD16- / NKp46+ human NK cell line KHYG-1 was assessed in a classical 4-h 51Cr-release assay in U-bottom 96 well plates. Daudi or B221 cells were labelled with 51Cr (50 μCi (1.85 MBq) / 1×106 cells), then mixed with KHYG-1 at an effector / target ratio equal to 50:1, in the presence of test antibodies at dilution range starting from 10−7 mol / L with 1 / 5 dilution (n=8 concentrations)
[0221]After brief centrifugation and 4 hours of incubation at 37° C., 50 μL of supernatant were removed and transferred into a LumaPlate (Perkin Elmer Life Sciences, Boston, Mass.), and 51Cr release was measured with a TopCount NXT bet...
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