Method of producing etching mask, etching mask precursor, and oxide layer, and method of manufacturing thin film transistor
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first embodiment
[0077]1. Etching Mask Precursor, Configurations of Etching Mask, and Method of Producing these
[0078]The “etching mask precursor” according to this embodiment is in a state where aliphatic polycarbonate (which may include inevitable impurities. The same shall apply hereafter) is dissolved in a certain solvent (typically an organic solvent). Further, the “etching mask” according to this embodiment is in a state (typically a “gel state”) where the solvent has been removed by heating the etching mask precursor thereof to an extent where it can be used for screen printing.
[0079]The etching mask precursor or etching mask according to this embodiment mainly includes aliphatic polycarbonate, but may include a compound, composition, or material other than aliphatic polycarbonate. It is noted that there is no particular limitation for the lower limit of the content of aliphatic polycarbonate in the etching mask precursor or etching mask, but the mass percentage of aliphatic polycarbonate to t...
experimental example 1
[0123]As examples of aliphatic polycarbonate, samples of the etching mask precursors in which at least one of 4 types of PPCs having different mass-average molecular weights was dissolved were prepared as shown in the following (1) to (10). It is noted that each of the following mass-average molecular weights represents values for aliphatic polycarbonate only.
[0124](1) Only a PPC having mass-average molecular weight of 30000 (hereinafter may also be referred to as “Sample A”)
[0125](2) Only a PPC having mass-average molecular weight of 90000 (hereinafter may also be referred to as “Sample B”)
[0126](3) A 1:1 mixture of Sample A and Sample B (hereinafter may also referred to as “Sample AB”)
[0127](4) Only a PPC having mass-average molecular weight of 230000 (hereinafter may also be referred to as “Sample C”)
[0128](5) Only a PPC having mass-average molecular weight of 590000 (hereinafter may also be referred to as “Sample D”)
[0129](6) A 1:1 mixture of Sample C and Sample D (hereinafter m...
experimental example 2
[0158]Next, in the following experiment, the inventors of this application measured the average length of drawn out strands (mm) and zero-shear viscosity (Pa·s) of the samples (1) to (10) used in experimental example 1.
[0159]In this experiment, first, regarding the average length of drawn-out strands (mm), a cylindrical bar made of polytetrafluoroethylene and having a diameter “D” of 2.9 mm was dipped in a collection of aliphatic polycarbonate, which had been formed using each sample, within a container. When the cylindrical bar was then raised at a velocity “v” of 5 mm / second, and then the length “L” (mm) of a strand drawn out from the outermost surface of the collection of the aliphatic polycarbonate was measured. In addition, the zero-shear viscosity η of each sample was measured using a rheometer (TA Instruments, AR-2000EX). Each of the above values was substituted as an evaluation parameter into the following formula for calculation.
“Evaluation parameter” (mm−1·Pa−1)=L / (D×v×η) ...
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