Producer of high-flux continuous homogeneous emulsion drop
A preparation device and high-throughput technology, applied in chemical instruments and methods, dissolution, mixers, etc., can solve the problems of continuous production difficulties, large power, particle size distribution, etc., and achieve the benefits of biological material activity and equipment The effect of small investment and low speed requirement
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Embodiment 1
[0026] Embodiment 1. High-throughput continuous uniform emulsion droplet preparation device prepares polylactic acid microspheres with uniform particle size (rotating speed 400rpm)
[0027] Pour 800mL of dichloromethane solution (oil phase) dissolved with 5g of polylactic acid (molecular weight: 100,000) into a 1000mL dispersed phase storage tank, and pump it into the device continuously, controlling the pressure at 1.2bar. 3200mL of 1.0wt% polyvinyl alcohol (PVA) deionized aqueous solution (water phase) was poured into the container continuously through the feed port (11). use figure 1 The shown high-throughput continuous uniform emulsion droplet preparation device (the outlet hole diameter is 1mm) prepares oil / water emulsion. The rotation speed of the belt runner is 400rpm, and the prepared emulsion is continuously output from the outlet (12). Then, the above obtained emulsion was stirred with a magnetic mechanical stirrer at 150 rpm for 5 hours to ensure complete volatili...
Embodiment 2
[0031] Embodiment 2. High-throughput continuous uniform emulsion droplet preparation device prepares polylactic acid microspheres with uniform particle size (rotating speed 300rpm)
[0032] Pour 800mL of dichloromethane solution (oil phase) dissolved with 5g of polylactic acid (molecular weight: 100,000) into a 1000mL dispersed phase storage tank, and pump it into the device continuously, controlling the pressure at 1.2bar. 3200mL of 1.0wt% polyvinyl alcohol (PVA) deionized aqueous solution (water phase) was poured into the container continuously through the feed port (11). use figure 1The shown high-throughput continuous uniform emulsion droplet preparation device (the outlet hole diameter is 1mm) prepares oil / water emulsion. The rotation speed of the belt runner is 300rpm, and the prepared emulsion is continuously output from the outlet (12). Then, the above obtained emulsion was stirred with a magnetic mechanical stirrer at 150 rpm for 5 hours to ensure complete volatiliz...
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