Quick solidification method for preparing non-crystalline thin band
A thin strip, amorphous technology, applied in the field of rapid solidification technology to prepare amorphous thin strips, can solve the problems of thin strips easily twisted together, limited strip length, short cooling time, etc. Quality, the effect of improving production efficiency
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Embodiment 1
[0020] Embodiment 1, prepare Zr-Al-Ni amorphous alloy, raw material is Zr-Al-Ni alloy through smelting, molten pool is a quartz tube, the inner diameter of cooling body copper is 1m, the outer diameter is 1.5m, and the diameter of rotating shaft is 0.5m.
[0021] The specific preparation process is:
[0022] (1) Put the Zr-Al-Ni alloy into the quartz tube, and adjust the position of the quartz tube;
[0023] (2) Vacuumize to a vacuum degree of 10 -4 Pa;
[0024] (3) Fill with pure argon to -0.5Pa;
[0025] (4) Turn on the speed knob and adjust the speed of the copper ring and the rotating shaft to 3000rpm and 6000rpm respectively;
[0026] (5) Heating to completely melt the alloy and spraying with pure argon;
[0027] (6) Let the rotating shaft contact the inner wall of the cooling body quickly, stick the thin strip, and pull the rotating shaft out of the cooling body.
Embodiment 2
[0028] Embodiment 2, preparation CaO-Al 2 o 3 Amorphous thin strip, the raw material is CaO and Al mixed uniformly and sintered 2 o 3 Powder, molten pool is α-Al 2 o 3 The inner diameter of the crucible, the copper cooling body, is 1m, the outer diameter is 1.5m, and the diameter of the rotating shaft is 0.5m. Such as figure 2 Prepare CaO-Al as shown 2 o 3 The process of amorphous ribbon is:
[0029] (1) Mix evenly CaO-Al 2 o 3 Put the block into the alumina crucible and adjust the position of the crucible;
[0030] (2) adjust the speed of the copper ring and the rotating shaft to be 4000rpm and 8000rpm respectively;
[0031] (3) heating to make CaO-Al 2 o 3 After complete melting, spray with gas;
[0032] (4) Let the rotating shaft contact the inner wall of the cooling body quickly, stick the thin strip, and pull the rotating shaft out of the cooling body.
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