Original composition of carbon material for electrode of electric double-layer capacitor
A technology of electric dipole and composition, which is applied in the direction of hybrid capacitor electrodes, hybrid/electric double layer capacitor manufacturing, electrolytic capacitors, etc., can solve the problem of insufficient performance of specific area, insufficient electrostatic capacitance, and insufficient performance, etc. problem, to achieve the effect of large electrostatic capacitance and small internal resistance
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Embodiment 1
[0085] (i) Manufacture of raw carbon composition
[0086] 10 vol% of residual oil from a vacuum distillation unit (0.17% by mass of sulfur component, 0.9% by mass of asphaltenes) was mixed with 90% by volume of bottom oil from a flow contact cracking apparatus of petroleum heavy oil. By carbonizing (coking) this heavy oil mixture at 500° C. for 1.0 hour, a raw carbon composition having a volatile content of 5.8% by mass and a microstrength of 7% was obtained. In addition, the structure of the raw carbon composition obtained in this way was observed by a polarizing microscope, and it was found that it was an optically anisotropic structure, and the flow pattern was the main factor. In addition, the average interlayer distance d of microcrystalline carbon 002 It is 0.346nm, and the porosity is 22%.
[0087] (ii) Manufacture of carbon materials
[0088] 200 parts by mass of potassium hydroxide was mixed with respect to 100 parts by mass of the raw material carbon composition, ...
Embodiment 2
[0098] The raw carbon composition of Example 1 was treated under an inert gas atmosphere at 650° C. for 1 hour to obtain a raw carbon composition with a volatile content of 3.3% by mass and a microstrength of 13%. In addition, the average interlayer distance of the microcrystalline carbon was 0.344 nm, and the porosity was 24%. Then, alkali activation treatment was performed in the same manner as in Example 1 to obtain a carbon material for electrodes. The carbon material has a specific area of 900m 2 / g, the micropore volume is 0.47cm 3 / g, the micropore diameter is 2.0nm. Using this carbon material, an electrode was produced in the same manner as in Example 1, a battery was mounted, and the capacitance was measured. As a result, the capacitance per unit volume (F / cc) was 34 F / cc.
Embodiment 3
[0100] The raw coke composition of Example 1 was treated under an inert gas atmosphere at 750° C. for 1 hour to obtain a raw coke composition with a volatile component of 1.7% by mass and a microstrength of 18%. In addition, the average interlayer distance of the microcrystalline carbon was 0.343 nm, and the porosity was 25%. Then, alkali activation treatment was performed in the same manner as in Example 1 to obtain a carbon material for electrodes. The carbon material has a specific area of 600m 2 / g, the micropore volume is 0.30cm 3 / g, the micropore diameter is 2.1nm. Using this carbon material, an electrode was produced in the same manner as in Example 1, a battery was mounted, and the capacitance was measured. As a result, the capacitance per unit volume (F / cc) was 35 F / cc.
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