Method of synthesizing cefixime

A synthesis method and technology of cefixime, applied in the field of cefixime, can solve problems such as poor quality and low yield, and achieve the effects of improving yield, improving quality and yield, and reducing material loss
CN101016305AInactive Publication Date: 2007-08-15河源市制药工程技术研究开发中心

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
河源市制药工程技术研究开发中心
Publication Date
2007-08-15
Estimated Expiration
Not applicable · inactive patent

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Abstract

The invention discloses a synthesizing method of cefuroxime, which is characterized by the following: crystallizing cefuroxime intermediate MECEF; synthesizing cefuroxime through water-phased extract of MECEF without dissolving MECEF; saving cost to improve receiving rate effectively; shortening manufacturing period.
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Description

technical field

[0001] The invention belongs to the technical field of cefixime in the chemical pharmaceutical industry, and in particular relates to a synthesis method of cefixime. Background technique

[0002] Cefixime is a third-generation oral cephalosporin antibiotic, which has a broad-spectrum antibacterial effect on Gram-positive and Streptococcus), pneumococcus and Escherichia coli, Moraxella, Neisseria gonorrhoeae, Proteus mirabilis, and Cathaeria in Gram-negative bacteria showed stronger bactericidal effect than other oral cephalosporins. It has the characteristics of broad spectrum, high efficiency, enzyme resistance and low toxicity, and is an anti-infection oral drug widely used in clinical practice.

[0003] The technical status of existing synthetic cefixime is as follows:

[0004] (1) In a reaction tank with a thermometer and a nitrogen device that has replaced air, add MICA (cefixime side chain acid), accelerator DM (dibenzothiazole disulfide), triphenylph...

Claims

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