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Technique for producing extractive of olive growing leaves

A technology of olive leaf extract and production process, which is applied in the field of production process of olive leaf extract, can solve the problems of low content of oleuropein, total phenols and flavonoids, etc., and achieve good product quality, high extraction rate and reasonable process route Effect

Inactive Publication Date: 2007-10-10
TIANYUAN OIL OLIVE TECH DEV LONGMAN
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] At present, there are reports in China that olive leaves and olive leaves are used to extract and process olive extracts, but most of them are directly spray-dried after water extraction or alcohol extraction. The content of oleuropein, total phenols and flavonoids in the product is low, which is significantly lower than the standards required by foreign countries. Extract content

Method used

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  • Technique for producing extractive of olive growing leaves

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] Take 100kg of dried olive leaves, crush them, add 10 times of 90% ethanol to reflux extraction, filter the leachate, concentrate in vacuum, and dry in vacuum. The temperature of concentration and drying should not exceed 55°C to obtain 16kg of crude olive leaf extract. The crude extract was pulverized, passed through a 80-mesh sieve, dissolved in water, filtered, separated by membrane, separated and purified by ion exchange, and 1.8 kg of olive leaf extract was obtained.

Embodiment 2

[0025] Take 100kg of dried olive leaves, crush them, add 15 times of 80% methanol to reflux and extract, filter the leachate, concentrate in vacuum, and dry in vacuum. The concentration and drying temperature should not exceed 55°C to obtain 13kg of crude olive leaf extract. The crude extract was pulverized, passed through a 60-mesh sieve, dissolved in water, filtered, separated by membrane, ion-exchanged and alcoholized to obtain 1.5 kg of olive leaf extract.

Embodiment 3

[0027] Take 100kg of dried olive leaves, crush them, add 10 times of 85% ethanol to soak and extract twice, each time for 48 hours, and the extraction temperature is 55°C, combine the extracts, filter, concentrate in vacuum, and dry in vacuum. The temperature of concentration and drying should not exceed 55°C, 19kg of crude olive leaf extract was obtained. The crude extract was pulverized, passed through a 80-mesh sieve, dissolved in water, filtered, separated by membrane, ion-exchanged and alcoholized to obtain 1.8 kg of olive leaf extract.

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Abstract

A process for preparing the extract of olive leaf includes such steps as low-temp drying in dark condition, pulverizing, extracting in ethanol or methanol by reflux, immersing, seeping, or ultrasonic wave, filtering, vacuum concentrating, vacuum drying to obtain coarse extract, pulverizing, sieving, dissolving in water, filtering, membrane separation, and purifying by ion exchange.

Description

technical field [0001] The invention relates to a production process of olive leaf extract. Background technique [0002] Olive, (Olea europaea L.), also known as foreign olive, European olive, and olean, is a plant of the genus Olea L in the family Oleaceae, and is a world-renowned evergreen tree species for oil and fruit. Olives are native to Asia Minor, and are mainly distributed in the Mediterranean coastal areas, with Spain, Italy, Portugal and Albania as the concentrated production areas. When Premier Zhou Enlai visited Albania in 1964, he decided to introduce and promote olive oil after learning about its special efficacy and wide application. After decades of hard work by our country's olive introduction experts, the introduction has been successful. The olive production in suitable areas has reached the level of origin. According to incomplete statistics, my country's existing olive area is about 400,000 mu (10 million plants). [0003] Olive is a traditional me...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K36/185A61P9/06A61P3/06A61P3/10A61P29/00A61P31/10A61P37/04A61P39/06A61K127/00
Inventor 姚自奇温凯白小勇付军
Owner TIANYUAN OIL OLIVE TECH DEV LONGMAN
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