Cubic boron nitride compact
A technology of powder and composition, which is applied in the field of preparation of powder composition, and can solve problems such as tool failure, aggravation, and limited tool life
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Embodiment 1
[0049] TiC 0.8 Mixed with Al powder, of which TiC 0.8 The weight ratio to Al powder is 90:10. The powder mixture was heated to 1025°C under vacuum for 30 minutes, and then crushed and made into powder. The powder mixture was pulverized with a hexane sand mill for 4 hours. Keep the solid / liquid ratio at 14.3% by volume. CBN powder with an average particle size of 1.2 microns was added in a ratio such that 50% by volume of CBN was obtained in the mixture, and then the mixture was sand-milled and pulverized for 1 hour. Keep the solid / liquid volume ratio at 20% by volume. After sand milling, the slurry is dried under vacuum and formed into briquettes.
[0050] The ground powder contained about 2.01 wt% tungsten carbide from sand milling, which was measured by the weight difference of the grinding media before and after sand milling.
[0051] The material was sintered at 55 kbar and 1300°C to prepare a CBN compact. The X-ray analysis of the CBN compact showed the FWHM peak broadening e...
Embodiment 2
[0063] Put Ti(C 0.5 N 0.5 ) 0.8 Mixed with Al powder, where Ti(C 0.5 N 0.5 ) 0.8 The weight ratio to Al powder is 90:10. The powder mixture was heated to 1025°C under vacuum for 30 minutes, and then crushed and made into powder. The powdery mixture was pulverized with a hexane sand mill for 4 hours. Keep the solid / liquid ratio at 15.3% by volume. CBN powder with an average particle size of 0.7 microns was added in a ratio such that 50% by volume of CBN was obtained in the mixture, and then the mixture was sand-milled and pulverized for 1 hour. Keep the solid / liquid volume ratio at 18.3% by volume. After sand milling, the slurry is dried under vacuum and formed into briquettes.
[0064] The ground powder contained about 1.1 wt% tungsten carbide from sand milling, which was measured by the weight difference of the grinding media before and after sand milling.
[0065]The material was sintered at 55 kbar and 1300°C to produce CBN compacts. The X-ray analysis of the CBN compact showed...
Embodiment 3
[0081] The substoichiometric titanium carbonitride powder with an average particle size of 1.4 microns (Ti(C 0.3 N 0.7 ) 0.8 ) Is mixed with Al powder with an average particle size of 5 microns. Ti(C 0.3 N 0.7 ) 0.8 The mass ratio to Al is 90:10. The powder was mixed and pressed into a titanium cup to form a compact, and heated to 1025° C. for 30 minutes under vacuum and then crushed and ground into powder. The powder mixture was subsequently sand-milled for 4 hours. In the first stage of grinding, the solid / liquid ratio was maintained at 15.1% by volume. A CBN powder mixture containing about 30% by weight of CBN with an average particle size of 0.7 microns and other CBN with an average particle size of 2 microns was added to the slurry in a certain amount to obtain a total CBN of 60% by volume. Grind and mix the CBN-containing slurry by sand milling for 1 hour. In the second stage of grinding, the solid / liquid ratio was maintained at 18.3% by volume. The slurry was dried under va...
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