Anti-bleeding, anticoagulated colloid for textile decoration printing and preparation thereof
An anti-gelling agent and a technology for textiles, used in the field of anti-seepage and anti-gelling agents for textile printing, can solve the problems of inability to achieve color fixing effect and lack of versatility, and improve the fluidity of printing paste and improve uniformity. The effect of dyeing and preventing plaque
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Embodiment 1
[0021] (1) Neutralization reaction: add 171KG of methacrylic acid, 86KG of sodium vinylbenzenesulfonate, 18KG of 2-acrylamido-2-methylpropanesulfonic acid, and 51KG of acrylic acid in a stainless steel kettle, with a mass percentage concentration of 20%. Neutralize with 332KG of ammonia water, keep the temperature at 0-40°C, and adjust the pH value of the product to 6.0-7.0;
[0022] (2) Emulsification reaction: Add 51KG of oil (200-300 distillation range), 19KG of sorbitan monooleate, 2KG of diallyl phthalate, and 0.4KG of modified silicone linear in the emulsification reaction kettle , while stirring at high speed, add the neutralizing solution completely, and finally add 220KG of water to make it fully emulsified at a temperature of 40-50°C for 30 minutes;
[0023] (3) Polymerization reaction: heat up to 65°C, add 0.15KG of initiator sodium persulfate dropwise, make it polymerize at 65-70°C for 1 hour, then cool down to 30-40°C, add ethoxylated nonyl Phenol ether (HLB=12.3...
Embodiment 2
[0025] Raw material ratio methacrylic acid 179KG, sodium vinylbenzene sulfonate 89KG, 2-acrylamido-2-methylpropanesulfonic acid 20KG, acrylic acid 54KG, use mass percent concentration to be 20% ammonia water 338KG, oil (distillation range is 200 -300°C) 59KG, sorbitan monooleate 21KG, diallyl phthalate 4KG, amino-modified silicone linear 0.6KG, ethoxylated nonylphenol ether (HLB=12.3) 4KG, Sodium persulfate 0.16KG water 250KG, the technological process of production is with embodiment 1.
Embodiment 3
[0027] Raw material ratio 172KG of methacrylic acid, 87KG of sodium vinylbenzene sulfonate, 18.5KG of 2-acrylamido-2-methylpropanesulfonic acid, 52KG of acrylic acid, 20% ammonia water 334KG with mass percent concentration, oil (distillation range is 200-300℃) 53KG, sorbitan monooleate 18.5KG, diallyl phthalate 2.5KG, amino-modified silicone linear 0.35KG, ethoxylated nonylphenol ether (HLB=12.3 ) 3.5KG, sodium persulfate 0.154KG water 230KG, the technological process of production is with embodiment 1.
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