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Reactive dye composition and preparing process and application thereof

A technology of reactive dyes and compositions, applied in dyeing methods, organic dyes, textiles and papermaking, etc., can solve the problems of increased dyeing cost for customers, unsatisfactory washing fastness, low alkali resistance stability, etc., and achieves excellent color fixing rate. , good washing fastness, improving the effect of chlorine fastness and light fastness

Inactive Publication Date: 2008-03-19
ZHEJIANG RUIHUA CHEM
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Now most of them use active red, yellow and blue dyeing black containing dichloro-s-triazine and vinyl sulfone dual active groups. The sensitivity to alkali, the influence on bath ratio and the sensitivity to temperature all have certain differences, so the color reproducibility of dyeing is poor, and the chance of rework is great, resulting in a substantial increase in dyeing costs for customers
The black dyed by the combination of common red, yellow and blue reactive dyes has unsatisfactory washing fastness; the current black dyes suitable for cold pad batch generally have low alkali resistance stability, low color fixation rate, Problems such as poor fastness
Although the dye combinations disclosed in CN-1063468C and CN-1322064C have improved the compatibility of dyes to a certain extent, and have improved level dyeing and carving whiteness, but in dyeing depth and dyed nylon cotton blending There are still defects such as severe staining of nylon parts in the fabric, so it still cannot meet the needs of printing and dyeing factories when dyeing very dark colors

Method used

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  • Reactive dye composition and preparing process and application thereof
  • Reactive dye composition and preparing process and application thereof
  • Reactive dye composition and preparing process and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0057] Prepare dyes in the following proportions:

[0058]60% A1, 12% B1, 11% C2, 3% D1, and the rest are additives, and the prepared composition is P1. The preparation method is to grind (A1) compound, (B1) compound, (C2) compound, (D1) compound and 8% sodium sulfate, 5% dispersant MF and 1% dustproof agent AC-805, and then Use a mixer for mixing. The mixer can be cone-shaped, drum-type, or pear-knife-type. After mixing evenly, test and analyze the qualified package.

Embodiment 2

[0060] Prepare dyes in the following proportions:

[0061] 60% A1, 6% B2, 13% C2, 3% D1, and the rest are additives (10% sodium bicarbonate, 5% dispersant MF, 1% dustproof agent AC-805 and 2% urea). The composition is P2, and the preparation method is the same as in Example 1.

Embodiment 3

[0063] Prepare dyes in the following proportions:

[0064] 54% A1, 12% B3, 19% C1, 3% D1, and the rest are additives, and the prepared composition is P3. The preparation method is to produce the compound slurry of formula (A1), formula (B3), formula (C1) and formula (D1) and 8% dye accelerator sodium sulfate, 3.5% dispersant MF and 0.5% dustproof The agent AC-805 is poured into the color storage tank with stirring in proportion, and the mixer is started to stir evenly. After passing the test, it is directly packaged to make a liquid product, or dried through a spray tower, drying room, flash evaporation, etc. to obtain a granular or powder product.

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Abstract

The invention discloses an active dye composition, which includes compound as showed in formula (A), formula (B), formula (C) and formula (D) and additive. 4 components of the active dye composition of the invention active dye composition are medium temperature dye, wherein the oil-water ratio, dye curve, affinity to cellulose, degree of dyeing, color fixing rate, sensitivity to salt and base, effect on bath ratio and sensitivity to temperature are very close. The composition has good dyeing synchronism and level dyeing property, and much higher color fixing rate, thereby being applicable for dip dyeing, continuous dyeing, cold dome, and printing and embossing of cellulose or protein fiber.

Description

1. Technical field [0001] The invention relates to a reactive dye composition and its preparation method and application, more particularly to a reactive dye composition suitable for cellulose and protein fibers and its preparation method and application method. 2. Background technology [0002] In the dyeing of cellulose fibers, dyeing black with common red, yellow and blue reactive dyes is more likely to produce cylinder difference. Now most of them use active red, yellow and blue dyeing black containing dichloro-s-triazine and vinyl sulfone dual active groups. The sensitivity to alkali, the influence on the bath ratio and the sensitivity to temperature all have certain differences, so the color reproducibility of dyeing is poor, and the chances of repair are great, resulting in a substantial increase in dyeing costs for customers. The black dyed by the combination of common red, yellow and blue reactive dyes has unsatisfactory washing fastness; the current black dyes sui...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09B67/24D06P1/38D06P3/66
Inventor 杨国旗赵国生吴清和柳长江
Owner ZHEJIANG RUIHUA CHEM
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