Curing colouration composition, color filtering device and liquid crystal display using the color filtering device
A coloring composition, a curable technology, applied in photosensitive materials, instruments, nonlinear optics, etc. for optomechanical equipment, which can solve problems such as performance degradation, insufficient pigment dispersion, and clogging of inkjet nozzles
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[0561] -Preparation of curable coloring composition-
[0562] The curable coloring composition of the present invention is prepared by mixing a colorant, the acrylic copolymer (alkali-soluble resin) of the present invention, a polymerizable compound, a photopolymerization initiator, and other components (preferably together with a solvent) as needed, and use It is prepared by mixing and dispersing in various mixers or dispersing machines.
[0563] In addition, the step of mixing and dispersing (mixing and dispersing step) is preferably constituted by kneading and dispersion followed by a micro-dispersion treatment, and the kneading and dispersion may be omitted. In addition, the type of pigment used in the kneading and dispersion step is preferably made finer in particle size by a salt kneading method or the like. The method of mixing table salt is known in Patent No. 3130217, JP 2003-504480, etc. In addition, pigments of fine particles formed by an aggregation method can also be ...
Example Embodiment
[0601] [Example 1]
[0602]
[0603] "1. Preparation of red curable composition"
[0604] The following red composition A was stirred for 1 hour using a homogenizer under the condition of 3000 rpm. The resultant mixed solution was subjected to a micro-dispersion treatment for 4 hours by a bead disperser (trade name: ディスパ一マット, manufactured by GETZMANN) using 0.3 mm zirconia beads to obtain a dispersion. In addition, the average particle diameter of the pigment is measured by a usual method by SEM observation.
[0605] -Red composition A-dispersion
[0606] ·Pigment: Pigment Red 254 (average particle size 20nm) 11 parts
[0607] ·Pigment: Pigment Red 177 (average particle size 18nm) 4 parts
[0608] · Dispersing resin (B-1-3) (the following structure) 5 parts
[0609] · Dispersing agent (trade name: Disperbyk-161, manufactured by ビックケミ一社) 3 parts
[0610] 3 parts of mixed solvent of methoxybutyl acetate and butyl acetate
[0611] ·Alkali-soluble resin: benzyl methacrylate / methacryl...
Example Embodiment
[0630] [Example 2]
[0631] "Preparation of green curable composition"
[0632] The red composition A of Example 1 was replaced with the following green composition A to obtain a dispersion.
[0633] -Green composition A-dispersion
[0634] ·Pigment: Pigment Green 36 (average particle size 19nm) 11 parts
[0635] ·Pigment: Pigment Yellow 150 (average particle size 22nm) 7 parts
[0636] · Dispersing resin (B-1-26) (the following structure) 5 parts
[0637] · Dispersing agent (trade name: Disperbyk-161, manufactured by ビックケミ一社, 30%
[0638] 3 solutions)
[0639] ·Alkali-soluble resin: benzyl methacrylate / methacrylic acid copolymer
[0640] 4 parts = 75 / 25 [mass ratio] copolymer, propylene glycol monomethyl ether acetate solution with weight molecular weight Mw: 5000 (solid content: 50% by mass)
[0641] ·(B) Solvent for dissolving dispersion resin: Methyl 3-ethoxyprop...
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