Pharmaceutical composition of cattail pollen and kudzu root
A composition, technology of kudzu root extract, applied in the field of medicine
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Embodiment 1
[0100] The preparation of embodiment 1 Puhuang extract (with total flavonoids as main component)
[0101] 1. Preparation of Puhuang Extract
[0102] Take the medicinal material of Puhuang, add 70% ethanol to extract three times, and extract for 3 hours each time. Add alcohol 14 times the amount for the first and second times, add alcohol 10 times the amount for the third time. Combine the extracts, filter, recover ethanol from the filtrate to a relative density of 1.04-1.06 (50°C), add an equal amount of water to dilute, mix well, refrigerate at 4°C for 24 hours, centrifuge, take the supernatant, shake with an equal amount of petroleum ether Shake and extract twice, discard the petroleum ether solution, shake and extract the water solution three times with an equal amount of water-saturated n-butanol, combine the n-butanol extracts, concentrate to a thick paste, and spray dry to obtain the Puhuang extract.
[0103] 2. Determination of the content of Puhuang extract
[010...
Embodiment 2
[0112] The preparation of embodiment 2 kudzu root extract (with total flavonoids as main component)
[0113] 1. Preparation of kudzu root extract
[0114] Take Pueraria root medicinal material, pulverize, add 75% ethanol to heat and reflux for extraction 3 times, add 12 times the amount of alcohol for the first time, extract for 2 hours, add 10 times the amount of alcohol for the second time, extract for 2 hours, add 8 times the amount of water for the third time, Extract for 1.5 hours. Combine the extracts, filter, the filtrate is concentrated until it has no alcohol smell, filter, and the processed D on the filtrate 101 In the macroporous resin, elute with water, 15% ethanol, and 70% ethanol respectively, and the elution volume is 3 times the volume of the column. Collect 70% of the eluate, recover ethanol, and concentrate under reduced pressure to a relative density of 1.1-1.3 (50°C) and dried to obtain the kudzu root extract.
[0115] 2. Determination of Pueraria root...
Embodiment 3
[0124] Embodiment 3: the preparation of pueraria tablet
[0125] 1. Prescription:
[0126] Prescription 1
[0127] Puhuang 20g (equivalent to 1000g of raw medicinal materials)
[0128] Pueraria 60g (equivalent to 2000g of raw medicinal materials)
[0129] Starch 120.0g
[0130] Microcrystalline Cellulose 40.0g
[0131] 2% HPMC aqueous solution appropriate amount
[0132] Magnesium Stearate 2.0g
[0133] Sodium starch glycolate 4.0g
[0134] A total of 1000 tablets were prepared
[0135] Prescription 2
[0136] Puhuang 40g (equivalent to 2000g of raw medicinal materials)
[0137] Pueraria 120g (equivalent to 4000g of raw medicinal materials)
[0138] Starch 140.0g
[0139] Microcrystalline Cellulose 40.0g
[0140] 2% HPMC aqueous solution appropriate amount
[0141] Magnesium Stearate 2.0g
[0142] Sodium starch glycolate 4.0g
[0143] A total of 1000 tablets were prepared
[0144] Prescription 3
[0145] Puhuang 60g (equivalent to 3000g of raw medicinal mate...
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