Fish meat petroleum hydrocarbon content determination method
A technology of petroleum hydrocarbon content and determination method, which is applied in the field of food
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[0129] Example 1 Determination of petroleum hydrocarbon content in silver carp
[0130] Perform the measurement according to the following steps:
[0131] 1. Fish processing steps
[0132] The silver carp purchased from Qingshan Market is scaled, peeled, and then the meat is taken, and then mashed and mixed with a JJ-2 tissue mashing homogenizer produced by Jiangsu Changzhou Guohua Instrument Factory, and the obtained fish paste is placed in a sealed container. Store in a glass bottle at a temperature of -20°C for later use.
[0133] 2. Saponification of fish
[0134] Thaw the fish paste obtained in step (1), weigh 2.5 g of fish paste into an iodine measuring flask, and add 15 ml of 5mol / L analytically pure sodium hydroxide solution (deionized water, in line with GB / T 6682 standard level 1 water , Sinopharm Chemical Preparation Co., Ltd.), adding 20 mL of absolute ethanol, shaking and saponifying at 30°C for 20 hours to prepare fish digestion.
[0135] 3. Extraction and adsorption...
Example Embodiment
[0156] Example 2 Determination of petroleum hydrocarbon content in grass carp
[0157] Follow the steps below to determine:
[0158] 1. Fish processing steps
[0159] The grass carp purchased from Qingshan Market is descaled and peeled, and then the meat is taken, and then mashed and mixed with the JJ-2 tissue mashing homogenizer produced by Jiangsu Changzhou Guohua Instrument Factory. The obtained fish paste is placed in a sealed glass bottle Medium, keep it at -20℃ for later use.
[0160] 2. Saponification of fish
[0161] Thaw the fish paste obtained in step (1), weigh 2.8g of fish paste into an iodine measuring flask, and add 15 mL of 6mol / L analytically pure sodium hydroxide solution (deionized water, in line with GB / T 6682 standard level 1 water , Sinopharm Chemical Preparation Co., Ltd.), adding 15 mL of absolute ethanol, shaking and saponifying at 30°C for 20 hours to prepare fish digestion.
[0162] 3. Extraction and adsorption
[0163] Pour 100 mL of the fish digestion s...
Example Embodiment
[0176] Example 3 Determination of petroleum hydrocarbon content in squid
[0177] Follow the steps below to determine:
[0178] 1. Fish processing steps
[0179] The squid purchased from Qingshan Market is taken from its meat, and then mashed and mixed with a JJ-2 tissue mashing homogenizer produced by Jiangsu Changzhou Guohua Instrument Factory. The obtained fish paste is placed in a sealed glass bottle at a temperature of -20 Store at ℃ for later use.
[0180] 2. Saponification of fish
[0181] Thaw the fish paste obtained in step (1), weigh 2.3 grams of fish paste into an iodine measuring flask, and add 20 mL of 6mol / L analytically pure sodium hydroxide solution (deionized water, in line with GB / T 6682 Grade 1 water standard , Sinopharm Chemical Preparation Co., Ltd.), adding 15 mL of absolute ethanol, shaking and saponifying at 35°C for 18 hours to prepare fish digestion.
[0182] 3. Extraction and adsorption
[0183] Pour 100 mL of the fish digestion solution obtained in step...
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