Micro-wave sintering method for foam glass

A microwave sintering and foam glass technology, which is applied in glass forming, glass production, glass manufacturing equipment, etc., can solve the problems of large temperature difference inside and outside the foam glass body, small heat radiation and air convection, poor sintering and foaming quality, etc., to achieve The effect of shortening the sintering time, good foaming quality and improving sintering quality

Inactive Publication Date: 2008-09-17
SHAANXI UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The traditional sintering of foam glass is to heat the glass body through heat radiation and air convection, but due to the uneven heat radiation and the small air convection in the gaps in the foam glass body, the inside and outside of the foam glass body during the sintering process The large temperature difference leads to the problem of poor sintering and foaming quality
[0003] Microwave sintering, as an efficient heating method, has the advantages of wide application range, high energy utilization rate, no pollution, and simultaneous internal and external sintering. For example, it is used for sintering of foam glass body to solve its uneven sintering and poor foaming quality. , low thermal efficiency and other issues, it will be a good way

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0008] Embodiment 1: First, the foam glass batch is dry-pressed under a pressure of 7Mpa to form a green body, then the foam glass green body is put into a clay mold, and the mold and the foam glass green body are placed together and the pressure is 1.0× 10 5 Pascal's oxidizing atmosphere or neutral atmosphere industrial batch microwave bell jar furnace, in which the microwave frequency is 915MHz, the green body is heated to 300°C within 5 minutes, and the temperature is raised to 300°C within 30 minutes after constant temperature for 10 minutes. 750°C, keep warm for 40 minutes, then turn off the microwave source, and quickly cool down to 600°C within 5 minutes, keep the temperature for 20 minutes, and then cool to room temperature with the furnace. Measure the temperature with an infrared thermometer. After being released from the furnace, after inspection, the sintered product is qualified if it meets the design requirements, has a high-quality appearance, and is 100°C lowe...

Embodiment 2

[0009] Embodiment 2: First, the foam glass batch material is dry-pressed under a pressure of 7Mpa to form a green body, then the foam glass green body is put into a clay mold, and the mold and the foam glass green body are placed together and the pressure is 1.0× 10 5 In an industrial batch microwave bell jar furnace with an oxidizing atmosphere or a neutral atmosphere in Pascal, where the microwave frequency is 300MHz, the green body is heated to 350°C within 5 minutes, and the temperature is raised to 350°C within 40 minutes after constant temperature for 10 minutes. 780°C, keep warm for 30 minutes, then turn off the microwave source, and quickly cool down to 600°C within 5 minutes, keep the temperature for 20 minutes, and then cool to room temperature with the furnace. Measure the temperature with an infrared thermometer. After being released from the furnace, after inspection, the sintered product is qualified if it meets the design requirements, has a high-quality appear...

Embodiment 3

[0010] Embodiment 3: First, the foam glass batch material is dry-pressed under a pressure of 7Mpa to make a green body, then the foam glass green body is put into a clay mold, and the mold and the foam glass green body are placed together and the pressure is 1.0× 10 5 In an industrial batch microwave bell jar furnace with an oxidizing atmosphere or a neutral atmosphere, the microwave frequency is 500MHz, so that the green body is heated to 320°C within 5 minutes, and the temperature is raised to 320°C within 45 minutes after constant temperature for 10 minutes. 820°C, keep warm for 15 minutes, then turn off the microwave source, and quickly cool down to 600°C within 5 minutes, keep the temperature for 20 minutes and then cool to room temperature with the furnace. Measure the temperature with an infrared thermometer. After being released from the furnace, after inspection, the sintered product is qualified if it meets the design requirements, has a high-quality appearance, and...

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PUM

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Abstract

A microwave sintering method of foam glass comprises the following steps of: placing a foam glass blank into a microwave sintering device with oxidizing atmosphere or neutral atmosphere and microwave frequency of 300MHz-300GHz, heating up to 300-350 DEG C in 5 min, keeping at the temperature for 10 min, heating up to 750-820 DEG C in 20-45 min, keeping at the temperature for 15-40 min, turning off microwave source, rapidly cooling to 600 DEC G in 5 min, keeping at the temperature for 20 min, cooling to room temperature, and taking out. In the inventive method, the heat for microwave sintering is originated from inside, the foam glass blank is self-sintered by absorbing microwave, the internal and external temperature difference of the foam glass blank is small during sintering process, so as to uniformly sinter the foam glass blank, reduce sintering temperature, shorten sintering time, and improve sintering quality. The used temperature is 5-150 DEG C lower than conventional sintering temperature.

Description

technical field [0001] The invention relates to a preparation method of foam glass, in particular to a microwave sintering method of foam glass, belonging to a new foam glass sintering process. Background technique [0002] Foam glass is a new type of environmentally friendly building material with superior performance in heat insulation, sound absorption, moisture resistance, waterproof and light weight. The traditional sintering of foam glass is to heat the glass body through heat radiation and air convection, but due to the uneven heat radiation and the small air convection in the gaps in the foam glass body, the inside and outside of the foam glass body during the sintering process The large temperature difference leads to the problem of poor sintered foaming quality. [0003] Microwave sintering, as an efficient heating method, has the advantages of wide application range, high energy utilization rate, no pollution, and simultaneous internal and external sintering. For...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C03B19/06C03C11/00
CPCY02P40/57
Inventor 郭宏伟高档妮赵彦钊刘新年高淑雅付定军张军军刘诗林
Owner SHAANXI UNIV OF SCI & TECH
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