Method for extracting lignosulphonate from sodium sulfite bamboo pulp waste liquor

A technology of lignosulfonate and sodium sulfite, which is applied in the direction of lignin derivatives, chemical instruments and methods, and wastewater treatment in processing, etc., which can solve the problems of lignosulfonate with many impurities, affecting normal use, and easy to be damp and sticky, etc. problem, to achieve the effect of advanced environmental protection

Inactive Publication Date: 2008-10-01
四川省高县华盛纸业有限公司
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AI Technical Summary

Problems solved by technology

[0006] The biggest difference between red liquor and acid process wood raw material waste liquor is that it contains more degradation products of hemicellulose xylan, and the average molecular weight of the main components of lignosulfonate and polysaccharide materials in red liquor is higher than that of acid method The similar substances in the waste liquid of woody raw materials are much lower, so the red liquid used for the production of lignosulfonate must be purified in advance, otherwise, the produced lignosulfonate has too many impurities and is very easy to be damp and sticky , affecting normal use

Method used

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Embodiment

[0017] The red liquid is passed through a sieve to remove small fibers, and the mesh number of the sieve is 80, which is stored in the red liquid storage tank, and then the red liquid is pumped out from the red liquid storage tank, and then enters the filter to remove miscellaneous cells, solid impurities, microparticles, etc.,

[0018] Then the red liquid is sent to the purification and separation system, using artificially synthesized organic or inorganic film media, with external energy (such as: pressure difference, potential difference) as the driving force, using cross-flow circulation through the membrane to treat specific organic substances or Selective separation of inorganic substances, that is, through low molecular weight and high molecular interception, high molecular weight can be separated, purified, concentrated and enriched. The part of the feed liquid that is intercepted by the membrane becomes the concentrate, and the part that is permeated by the membrane b...

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Abstract

The invention relates to a method for extracting lignin-sulphonate from the waste solution of sodium sulfite bamboo pulp, which is characterized in that: red liquor is filtered for removing fibrils by a sieve; the filtered red liquor is delivered into a filtering machine for removing parenchyma cells, solid impurities and particles; then the red liquor is delivered into a purification and separation system for eliminating inorganic salt, organic carboxylate, small molecular saccharides substances and small molecular lignin-sulphonate; the purified red liquor is concentrated to proper concentration after evaporation; the concentrated red liquor can be directly or added with material to be put into a drying system for becoming dry powder, thus obtaining a finished product. The method has the advantages that the method solves problems interfering in the development of paper making enterprises of China that uses a sulphite method for pulping, provides an effective implementation technical proposal and builds a production line with advanced environmental friendliness, typicality and practicability, which contributes to the waste solution treatment and discharge of the paper making industry of China.

Description

Technical field [0001] The invention relates to a treatment method for waste liquid treatment and discharge of sodium sulfite pulping enterprises. Background technique [0002] The pulping and cooking method (sulfite method) has been used in the paper industry, including acid sulfite method, neutral sulfite method and alkaline sulfite method. The mainstream treatment method for the waste liquid is to concentrate and burn the waste liquid to recover alkali and heat energy. However, at this stage, domestic sodium sulfite cooking waste liquor is not suitable for alkali recovery. The reason is that the annual output of domestic pulping enterprises using sodium sulfite method is below 100,000 tons, and it is not beneficial to use alkali recovery for small scale. What is more important is which compound is in Harmful gases such as carbon dioxide will be produced during combustion, which fails to achieve the purpose of recycling. [0003] Although the sulfite pulping method has b...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C07G1/00C02F9/08C02F103/28C08H7/00
Inventor 袁承华
Owner 四川省高县华盛纸业有限公司
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